ISSN:
1600-5767
Quelle:
Crystallography Journals Online : IUCR Backfile Archive 1948-2001
Thema:
Geologie und Paläontologie
,
Physik
Notizen:
Transmission Laue diffraction photographs can be recorded with short exposure times from stationary macromolecular and small-molecule crystals. With the use of a broad wavelength band a very large number of reflections is stimulated in a single `snapshot' of large regions of reciprocal space. Processing software has been developed which allows quantitation of the Laue data without resort to monochromatic data. The procedures have been developed and the software strategies optimized by using test data recorded on the SRS wiggler from a protein, pea lectin, and small-molecule crystals. These latter include an organic molecule, trimethyl-1H-2,1,3-benzophosphadiazine-4(3H)-thione 2,2-disulfide, referred to as BPD, and a rhodium complex, [Rh6(CO)14(dppm)], where dppm is Ph2PCH2PPh2, referred to as RHCOP. Monochromatic data were available for comparison.
Materialart:
Digitale Medien
URL:
http://dx.doi.org/10.1107/S0021889889006564
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