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  • 1990-1994  (2)
  • 42.50.Lc  (1)
  • Ion-pair extraction  (1)
  • 1
    Electronic Resource
    Electronic Resource
    Springer
    Applied physics 55 (1992), S. 233-241 
    ISSN: 1432-0649
    Keywords: 42.50.Dv ; 42.50.Lc ; 42.65.Ky
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract Broadband high level squeezing was clearly observed from 100 kHz to 80 MHz using crystals Ba2NaNb5O15 of 5 mm length, MgO:LiNbO3 of 19 mm length and KNbO3 of 5.8 mm length. Maximum noise reductions detected on a spectrum analyzer were −1.2 dB (−24%), −1.25 dB (−25%), and −1.8 dB (−34%) for the three crystals, respectively. The maximum squeezing is limited mostly by “optical index damage” of the parametric crystals. A detailed analysis of the beam parameters traced along the pump beam, squeezed vacuum, etc. is given. A detailed discussion on the evaluation of the initial squeezed level is given. A preliminary experiment with compressed laser pulses to avoid the optical damage is also described.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1612-1112
    Keywords: Column liquid chromatography ; Atmospheric pressure chemical ionization-mass spectrometry ; Dried yeast ; Thiamine ; Ion-pair extraction
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary High-performance liquid chromatography (HPLC) and high-performance liquid chromatography/atmospheric pressure chemical ionization-mass spectrometry (HPLC/APCI-MS) have been applied to the analysis of thiamine in dried yeast. Thiamine was extracted from dried yeast with isobutanol containing sodium 1-octanesulfonate as an ion-pairing agent and determined by HPLC on a reversed phase ODS column with UV detection at 254 nm. Response was linear in the range 25–300 μg/g of thiamine in dried yeast with a coefficient of variation in the reproducibility of 8.0%. Thiamine was recovered in good yield (109.2%, n=5). Identification of the thiamine peak was obtained by the mass spectrum using the HPLC/APCI-MS system. The utility of the selected ion monitoring technique using the HPLC/APCI-MS was also investigated. The results obtained by this method are in good agreement with those obtained by the thiochrome method [1].
    Type of Medium: Electronic Resource
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