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Methylene malonamide. I. Synthesis and reactivity of the monomer (1982)

Jasne, S. J. ; Haas, H. C. ; Moreau, R. D. ; [et al.]

New York : Wiley-Blackwell

Journal of Polymer Science: Polymer Chemistry Edition 20 (1982), S. 35-42

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ISSN: 0360-6376

Keywords: Physics ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The first confirmed synthesis of methylene malonamide (MeMal) is reported. This monomer was prepared by the thermal elimination or fluoride-ion-initiated elimination of trimethylsilyl chloride from α-chloro-α(trimethylsilyl-2-methyl) malonamide. Spectral data for the monomer are given. MeMal has been shown to be unstable in a variety of protic organic solvents, including water and alcohols, thus giving the appropriate (α-methyl) substituted malonamides. MeMal is stable in most aprotic solvents.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/pol.1982.170200104

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