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  • 1970-1974  (7)
  • 1
    Electronic Resource
    Electronic Resource
    Zur Reaktion des N.N′-Bis(trichlorphosphoranyliden)-sulfamids (1972)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 105 (1972), S. 1510-1514 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Reaction of N.N′-Bis(trichlorophosphoranylidene)sulfamideSO2(NPCl3)2 reacts with silylamines (CH3)3SiNHR (R = C2H5, C3H7, C4H9) in a molar ratio of 1 : 2 to give 1, 2 and 3, with (CH3)3SiNHCH3 in a molar ratio of 1 : 1 to give the cyclic compound 41,2). From SO2(NPCl3)2 and disilylamines the compounds 5 and 6 can be obtained. The reaction of SO2[NPCl2N(C2H5)2]22) with [(CH3)3Si]2NCH3yields the heterocyclic compound 7. - The i.r., mass, 1H and 31P n.m.r. spectra of these compounds are reported.
    Notes: SO2(NPCl3)2 reagiert mit Silylaminen (CH3)3SiNHR (R = C2H5, C3H7, C4H9) im Molverhältnis 1 : 2 zu 1, 2 und 3, mit (CH3)3SiNHCH3 im Molverhältnis 1 : 1 zu der cyclischen Verbindung 41,2). Aus SO2(NPCl3)2 und Disilyaminen konnten die Verbindungen 5 und 6 gewonnen werden. Schließlich ist aus SO2[NPCl2N(C2H5)2]22) und [(CH3)3Si]2NCH3 die cyclische Verbindung 7 zugänglich. - Die IR-, Massen- und 1H- bzw. 31P-NMR-Spektren dieser Verbindungen werden mitgeteilt.
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19721050506
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  • 2
    Electronic Resource
    Electronic Resource
    Oxohalogencyclothiazene (1972)
    Weinheim : Wiley-Blackwell
    Zeitschrift für die chemische Industrie 84 (1972), S. 1149-1150 
    Details
    ISSN: 0044-8249
    Keywords: Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ange.19720842310
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  • 3
    Electronic Resource
    Electronic Resource
    Zur Reaktion des N,N′-Bis(trichlorphosphoranyliden)sulfamids (1974)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 107 (1974), S. 3756-3760 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Reaction of N, N′-Bis(trichlorophosphoranylidene)sulfamideSO2(NPCl3)2 reacts with alcohols ROH (R=CH3, C2H5, C3H7, C6H5) in a molratio 1:2 to form 1, 2, 3 and 4. The compounds 5 and 6 could be obtained in polar solvents from 1 and 2 by transfer of alkyl groups. Finally the cyclic compounds 7 and 8 are accessible by the reaction of 5 and 6 and [(CH3)3Si]NCH3 in a molratio 1:1. The i.r., mass, 1H and 31P n.m.r. spectra of these compounds are reported.
    Notes: SO2(NPCl3)2 reagiert mit Alkoholen ROH (R=CH3, C2H5, C3H7, C6H5) im Molverhältnis 1:2 zu 1, 2, 3 und 4, Aus 1 und 2 konnten in polaren Lösungsmitteln durch Alkylwanderung die Verbindungen 5 und 6 gewonnen werden. Schließlich sind aus 5 und 6 und [(CH3)3Si]2-NCH3 im Molverhältnis 1:1 die cyclischen Verbindungen 7 und 8 zugänglich. Die IR-, Massen- und 1H-bzw. 31P-NMR-Spektren dieser Verbindungen werden mitgeteilt.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19741071205
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  • 4
    Electronic Resource
    Electronic Resource
    Zur Reaktion des 3,3-Dichlor-1,5,2,4,6,3-dithiatriazaphosphor(V)in-S,S-bis(oxidchlorids), eines Dioxodichlorcyclodithiazaphosphazens (1973)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 106 (1973), S. 2969-2974 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Reaction of 3,3-Dichloro-1,5,2,4,6,3-dithiatriazaphosphor(V)in-bis(oxidchloride), a DioxodichlorocyclodithiazaphosphazenThe title compound 1 reacts with amines like HNRR′ in a molratio 1:2 to form 2, 3, 4, 5 6 and 7. The compound 8 is formed as a mixture of cis, trans-isomers from 1 and fluorinating agens like SbF3 and AgF2. The space group and lattice parameters of 8, as well as the i.r.-, mass-, 1H-, 10F- and 31P-n.m.r. spectra of the compounds are reported.
    Notes: Die Titelverbindung 1 reagiert mit Aminen HNRR′ im Molverhältnis 1:2 zu 2, 3, 4, 5, 6 und 7. Aus 1 und Fluorierungsmitteln wie SbF3 und AgF2 ist die Verbindung 8 als cis, trans-Isomerengemisch zugänglich. - Die Raumgruppe und Gitterkonstanten von 8 sowie die IR-, Massen-, 1H-, 19F- und 31P-NMR-Spektren der Verbindungen werden mitgeteilt.
    Additional Material: 2 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19731060927
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  • 5
    Electronic Resource
    Electronic Resource
    Zur Reaktion des N.N′-Bis(trichlorphosphoranyliden)-sulfamids (1971)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 104 (1971), S. 3804-3809 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Reaction of N.N′-Bis(trichlorophosphoranylidene)sulfamideSO2(NPCl3)2 reacts with silylamines (CH3)3SiNR2 (R=CH3, C2H5) in a molar ratio of 1 : 2 to give 1 and 2, in a molar ratio of 1 : 4 to give 3. From 1 and disilylamines the cyclic compounds 6 and 7 can be obtained as a mixture of cis.trans-isomers. The reaction of SO2(NPCl3)2 with [(CH3)3Si]2 NC2H5 yields the heterocyclic compound 5.  -  The i.r., mass, 1H and 31P n.m.r. spectra of the above mentioned compounds are reported.
    Notes: SO2(NPCl3)2 reagiert mit Silylaminen (CH3)3SiNR2 (R=CH3, C2H5) im Moleverhältnis 1 : 2 zu 1 und 2, im Molverhältnis 1 : 4 zu 3. Aus 1 und Disilylaminen sind die cyclischen Verbindungen 6 und 7 als cis.trans-Isomerengemisch zugänglich. Schließlich konnte aus SO2(NPCl3)2 und [(CH3)3Si]2NC2H5 der Heterocyclus 5 gewonnen werden.  -  Die IR-, Massen- und 1H- bzw. 31P-NMR-Spektren dieser Verbindungen werden mitgeteilt.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19711041210
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  • 6
    Electronic Resource
    Electronic Resource
    Reaktionen des 3,3-Dichlor-1,5,2,4,6,3-dithiatriazaphosphor(V)-in-S,S′-bis(oxidfluorids), eines cyclischen Phosphornitrilsulfanurhalogenids (1974)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 107 (1974), S. 592-597 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Reactions of 3,3-Dichloro-1,5,2,4,6,3-dithiatriazaphosphor(V)in-S,S′-bis(oxide fluoride), of a Cyclic Phosphornitrilsulfanur Halogenide(NSOF)2NPCl2 reacts with ammonia in a molar ratio of 1:2 to give 1, with silylamines (CH3)3SiNHR (R=CH3, C2H5) in a molar ratio 1:1 to yield 2 and 3, and with (CH3)3SiNR2 (R=CH3, C2H5) to form 4 and 5. The reaction of (NSOF)2NPCl2 with disilylamines [(CH3)3Si]2NR (R=H, CH3, C2H5) yields the compounds 6, 7, and 8. The i.r., mass, 1H, 19F, and 31P n.m.r. spectra of the above mentioned compounds are reported.
    Notes: (NSOF)2NPCl21 reagiert mit Ammoniak im Molverhältnis 1:2 zu 1, mit Silylaminen (CH3)3SiNHR (R=CH3, C2H5) im Molverhältnis 1:1 zu 2 und 3, mit (CH3)3SiNR2 (R=CH3, C2H5) zu 4 und 5. Schließlich konnten aus (NSOF)2NPCl 2 und Disilylaminen [(CH3)3Si]2NR (R=H, CH3, C2H5) die Verbindungen 6, 7 und 8 isoliert werden. Die IR-, Massen- und 1H-, 19F-und 31P-NMR-Spektren dieser Verbindungen werden mitgeteilt.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19741070227
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  • 7
    Electronic Resource
    Electronic Resource
    OxohalocyclothiazenesBased on a lecture by T.-P. Lin at the IV. European Fluorine Symposium in Ljubljana, Yugoslavia, on September 1, 1972. (1972)
    Weinheim : Wiley-Blackwell
    Angewandte Chemie International Edition in English 11 (1972), S. 1095-1096 
    Details
    ISSN: 0570-0833
    Keywords: Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/anie.197210951
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