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  • Microbial activity  (2)
  • Pesticides  (2)
  • crystal structure  (2)
  • 13C NMR spectroscopy  (1)
  • Activation process  (1)
  • 1
    Electronic Resource
    Electronic Resource
    Dynamics of central nervous activation during motor imagination
    Amsterdam : Elsevier
    International Journal of Psychophysiology 9 (1990), S. 75-80 
    Details
    ISSN: 0167-8760
    Keywords: Activation process ; Electroencephalogram ; Heart rate ; Motor imagination ; Respiration cycle ; Skin conductance
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Medicine , Psychology
    Type of Medium: Electronic Resource
    URL: http://linkinghub.elsevier.com/retrieve/pii/0167-8760(90)90008-2
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  • 2
    Electronic Resource
    Electronic Resource
    S-(N-(Thiocarbamoyl)benzimido)-dithiocarbamidsäureester (1996)
    Springer
    Monatshefte für Chemie 127 (1996), S. 291-296 
    Details
    ISSN: 1434-4475
    Keywords: S-(N-(Thiocarbamoyl)benzimido)dithiocarbamic esters ; Synthesis ; 13C NMR spectroscopy ; Side reactions
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Summary The synthesis of the title compounds3 (R 1=R 2=C2H5;n-C4H9) by reactions of N-(N′,N′-diethylthiocarbamoyl)benzimidechloride (2) with sodiumdialkyldithiocarbamates (1) in acetone is described. The low yields (〈25%) are caused by the occurrence of side reactions. The structures of the compounds were confirmed by IR,1H and13C NMR, and mass spectroscopy. Side reactions were detected by13C NMR spectroscopy; the results are discussed.
    Notes: Zusammenfassung Die Synthese der Titelverbindungen3 (R 1=R 2=C2H5;n-C4H9) durch Reaktionen von N-(N′,N′-Diethylthiocarbamoyl)-benzimidoylchlorid (2) mit Natriumdialkyldithiocarbamaten (1) in Aceton wird beschrieben. Die niedrigen Ausbeuten (bis 25% d.Th.) sind durch Nebenreaktionen bedingt. Die Strukturen der Verbindungen werden durch IR-,1H-NMR-,13C-NMR-und Massenspektren bestätigt. Nebenreaktionen werden13C-NMR-spektroskopisch verfolgt und die Ergebnisse diskutiert.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00813794
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  • 3
    Electronic Resource
    Electronic Resource
    Soil organic matter composition and pesticide bonding in sandy soils in relation to groundwater protection in the Northwest German Lower Plain (1996)
    Springer
    Biology and fertility of soils 23 (1996), S. 266-272 
    Details
    ISSN: 1432-0789
    Keywords: Key words Soil organic matter ; Microbial activity ; Groundwater contamination ; Pesticides ; Spodic horizons ; Landscape planning
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Geosciences , Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Notes: Abstract In sandy gleyic soils with a low groundwater table under arboriculture in Northwest Germany, a wide variation of groundwater pollution by pesticides has been observed. We therefore examined data on microbial activity and soil organic matter composition by wet chemistry, cross-polarization magic-angle spinning and 13C nuclear magnetic resonance, and pyrolysis–field ionization mass spectromy. However, neither microbial activity nor the soil organic matter composition of cultivated topsoils explained the differences in xenobiotic leaching into the groundwater. Data from Anthrosols suggested that these soils have a higher capacity for pesticide bonding because of high amounts of aromatic and carboxylic C moieties in the soil organic matter. However, despite the same pesticide inputs and time of application, the leached output from these soils was higher than that from the Podzols. Initial data from subsoil investigations suggest that the presence of a spodic horizon most likely reduces groundwater pollution by pesticides. Studies to assess fixation capacity and desorption kinetics in Bh horison seem warranted.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00335954
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    Paper (German National Licenses)
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  • 4
    Electronic Resource
    Electronic Resource
    Soil organic matter composition and pesticide bonding in sandy soils in relation to groundwater protection in the Northwest German Lower Plain (1996)
    Springer
    Biology and fertility of soils 23 (1996), S. 266-272 
    Details
    ISSN: 1432-0789
    Keywords: Soil organic matter ; Microbial activity ; Groundwater contamination ; Pesticides ; Spodic horizons ; Landscape planning
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Geosciences , Agriculture, Forestry, Horticulture, Fishery, Domestic Science, Nutrition
    Notes: Abstract In sandy gleyic soils with a low groundwater table under arboriculture in Northwest Germany, a wide variation of groundwater pollution by pesticides has been observed. We therefore examined data on microbial activity and soil organic matter composition by wet chemistry, cross-polarization magic-angle spinning and 13C nuclear magnetic resonance, and pyrolysis-field ionization mass spectromy. However, neither microbial activity nor the soil organic matter composition of cultivated topsoils explained the differences in xenobiotic leaching into the groundwater. Data from Anthrosols suggested that these soils have a higher capacity for pesticide bonding because of high amounts of aromatic and carboxylic C moieties in the soil organic matter. However, despite the same pesticide inputs and time of application, the leached output from these soils was higher than that from the Podzols. Initial data from subsoil investigations suggest that the presence of a spodic horizon most likely reduces groundwater pollution by pesticides. Studies to assess fixation capacity and desorption kinetics in Bh horison seem warranted.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00335954
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    Paper (German National Licenses)
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  • 5
    Electronic Resource
    Electronic Resource
    3-Diethylamino-5-phenyl-1,2,4-diselenazolium-tetrachloroniccolat(II)  -  Synthese und Struktur (1992)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 617 (1992), S. 89-92 
    Details
    ISSN: 0044-2313
    Keywords: 3-Diethylamino-5-phenyl-1,2,4-diselenazolium-tetrachloroniccolate(II) ; 1,2,4-diselenazolium salt ; selenaheterocyclic cation ; synthesis ; crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: 3-Diethylamino-5-phenyl-1,2,4-diselenazolium-tetrachloroniccolate(II)  -  Synthesis and StructureBis-(N′, N′-diethyl-N-benzoylselenoureato)nickel(II) reacts with diphosgene in benzene to 3-diethylamino-5-phenyl-1,2,4-diselenazolium-tetrachloroniccolate(II). Its structure is confirmed by RKSA and ESCA. The compound consists of cations, which are planar fivemembered rings and of tetrahedral tetrachloroniccolate(II) anions. The complex is isomorphic with 3-diethylamino-5-phenyl-1,2,4-dithiazolium-tetrachloroniccolate(II).
    Notes: Bis-(N′, N′-diethyl-N-benzoylselenoureato)nickel(II) reagiert mit Diphosgen in Benzen zu 3-Diethylamino-5-phenyl-1,2,4-diselenazolium-tetrachloroniccolat(II), dessen Röntgenkristallstrukturanalyse und Röntgenphotoelektronenspektrum vorgestellt und interpretiert werden. Die Verbindung besteht aus 1,2,4-Diselenazolium-Kationen, die als planare Fünfringe vorliegen und aus tetraedrischen Tetrachloroniccolat(II)-Anionen. Sie ist zu 3-Diethylamino-5-phenyl-1,2,4-dithiazolium-tetrachloroniccolat(II) isomorph.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19926170114
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  • 6
    Electronic Resource
    Electronic Resource
    Gemischtligandenkomplexe mit N-Acyl-thioharnstoffen: Die Struktur des [N-(Morpholinothiocarbonyl)-benzamidato] (3-amino-2-cyano-n-butyl-dithiocrotonato)nickel(II)Professor Dietrich Mootz zum 60. Geburtstage gewidmet (1993)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 619 (1993), S. 1295-1299 
    Details
    ISSN: 0044-2313
    Keywords: Mixed ligand complexes ; N-acylthiourea complexes ; nickel(II) chelates ; crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Mixed Ligand Complexes of N-Acyl-thioureas: The Structure of [N-(Morpholinothiocarbonyl)-benzamidato] (3-amino-2-cyano-n-butyl-dithiocrotonato)nickel(II)The reaction of a solution of N-(morpholinothiocarbonyl)benzamide and 3-amino-2-cyano-n-butyl-dithiocrotonate with nickel(II)-acetate tetrahydrate yields the first mixed ligand complex of N-acyl-thioureas. Its structure has been determined by an X-ray structure analysis. The coordination geometry is square planar. Bond lengths and angles are in good agreement with those of other bis and tris N-acyl-thiourea chelates.
    Notes: Aus einer Lösung von N-(Morpholinothiocarbonyl)-benzamid und 3-Amino-2-cyano-dithiocrotonsäure-n-butylester konnte durch Umsetzung mit Nickel(II)-acetat-tetrahydrat der erste Gemischtliganden-komplex mit N-Acylthioharnstoffen synthetisiert werden. Seine Struktur wurde mittels Röntgenkristallstrukturanalyse bestimmt. Die Koordinationsgeometrie ist quadratisch-planar. Bindungslängen und -winkel im N-Acylthioharnstoff-Teil des Komplexes stimmen gut mit denen anderer Bis- und Tris-N-acyl-thioharnstoff-Chelatkomplexe überein.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19936190724
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