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Identification by GC/MS of 6-monoacetylmorphine as an indicator of heroin abuse (1989)

Kintz, P. ; Mangin, P. ; Lugnier, A. A. ; [et al.]

Springer

European journal of clinical pharmacology 37 (1989), S. 531-532

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ISSN: 1432-1041

Keywords: heroin ; 6-monoacetylmorphine ; capillary gas chromatography ; selected ion monitoring ; GC/MS

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology , Medicine

Notes: Summary A capillary gas chromatography mass spectrometry assay has been developed for the determination of 6-monoacetylmorphine in human urine, which is a confirmatory marker of heroin abuse. It was extracted with chloroform-isopropanol-n-heptane (50:17:33, v/v) from alkalinized samples (pH 9.2), using levallorphan as the internal standard. After derivatization with trifluoroacetic anhydride, the drugs were separated on a 25-m capillary column BP 10 and detected by selected ion monitoring.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00558138

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