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  • Chemistry  (3)
  • Ability to act  (1)
  • Azathioprine  (1)
  • Best. von Arsen in Biolog. Material  (1)
  • 1
    Electronic Resource
    Electronic Resource
    Ein gaschromatographischer Nachweis von 6-Mercaptopurin im Serum von immunsupprimierten Transplantationspatienten (1982)
    Springer
    Research in experimental medicine 181 (1982), S. 19-25 
    Details
    ISSN: 1433-8580
    Keywords: Gas chromatography ; Serum level ; Azathioprine ; 6-Mercaptopurine ; Immunosuppression
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Summary The knowledge of serum levels of azathioprine or its metabolite 6-mercaptopurine is important for the monitoring of the immunosuppressive therapy after kidney transplantation, especially when kidney function is low. For this reason, the work of Bailey et al. was modified. 6-Mercaptopurine was extracted from the serum with a mixture of isopropanol-ethylacetate (1:1 v:v), derivatized with trimethylaniliniumhydroxyde and measured gaschromatographically. Sulfhydryl-protecting reagents were added to prevent loss of substance. Oxyethyltheophylline was used as the internal standard. The extraction and clean-up method recovered 80% of the 6-mercaptopurine present, the lower limit of sensitivity was 20 ng/ml, i.e., ten times lower than that of Bailey et al. The method could be realized on eight patients treated with azathioprine, the half life of the drug was about 20–40 min within the first hour after i.v. application.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01850986
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  • 2
    Electronic Resource
    Electronic Resource
    Handlungsfähigkeit bei tödlichen oralen Intoxikationen mit Cyan-Verbindungen (1999)
    Springer
    Rechtsmedizin 9 (1999), S. 56-61 
    Details
    ISSN: 1434-5196
    Keywords: Key words Cyanogen compounds ; Lethal oral ; intoxication ; Ability to act ; Schlüsselwörter Cyan-Verbindungen ; Tödliche orale Intoxikation ; Handlungsfähigkeit
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine , Law
    Description / Table of Contents: Zusammenfassung Die Einschätzung der Handlungsfähigkeit eines tödlich Vergifteten kann bei der Tatrekonstruktion sehr bedeutsam sein, insbesondere bei der Frage „Selbst- oder Fremdbeibringung des Giftes“. Klinische Publikationen gehen hierauf kaum ein. Deshalb wurden 27 Fälle tödlicher oraler Intoxikationen mit Cyan-Verbindungen der rechtsmedizinischen Institute Würzburg, Hamburg, München, Berlin (FU), Tübingen, Essen und Leipzig, bei denen eine Aussage zur Handlungsfähigkeit des später Verstorbenen möglich war, sowie die dazugehörigen polizeilichen und staatsanwaltschaftlichen Akten unter dieser Fragestellung ausgewertet. Ergebnis: in der Mehrzahl der Fälle betrug die Handlungsfähigkeit nur wenige Sekunden bis maximal 1 bis 2 Minuten. Im Untersuchungsgut und in der Literatur kamen allerdings auch Fälle vor, bei denen die Handlungsfähigkeit über ca. 5 bis 10 min erhalten war. Die Ergebnisse der Arbeit sollen dem Gutachter als Leitlinie bei der Klärung einschlägiger Fälle dienen.
    Notes: Abstract An accurate assessment of the duration of the ability to act of a victim of lethal poisoning can be of crucial importance in reconstructing the cause of the poisoning, especially in determining whether the poison was taken by the victim or given by another. Clinical studies have scarcely dealt with this problem. We therefore investigated 27 cases of lethal oral intoxication with cyanogen compounds on file at the university institutes of forensic medicine in Würzburg, Hamburg, Munich, Berlin (Free University), Tübingen, Essen and Leipzig with regard to the victim’s postintoxication ability to act. In addition we examined the records of the respective police and prosecuters offices as well as the relevant literature. In most cases the ability to act lasted only a few seconds to a maximum of 1–2 min. However, in some of the 27 cases the ability to act lasted for 5–10 min, a finding which agrees with reports in the literature. The present study is intended to provide forensic expert witnesses with guidelines for clarifying similar cases of lethal oral intoxication.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/s001940050080
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  • 3
    Electronic Resource
    Electronic Resource
    Anwendung der Graphitrohrküvette zur Arsenbestimmung in biologischen Proben mit der Hydrid-AAS-Technik (1980)
    Springer
    Fresenius' Zeitschrift für analytische Chemie 304 (1980), S. 141-142 
    Details
    ISSN: 1618-2650
    Keywords: Best. von Arsen in Biolog. Material ; Spektrometrie, Atomabsorption ; Graphitrohrküvette, Hydridtechnik
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00474372
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  • 4
    Electronic Resource
    Electronic Resource
    Elektrostatische Behinderung der freien Drehbarkeit (1930)
    Weinheim : Wiley-Blackwell
    Zeitschrift für die chemische Industrie 43 (1930), S. 747-749 
    Details
    ISSN: 0044-8249
    Keywords: Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ange.19300433404
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  • 5
    Electronic Resource
    Electronic Resource
    Des wahren Sicherheitszündholzes Eigenheiten (1909)
    Weinheim : Wiley-Blackwell
    Zeitschrift für die chemische Industrie 22 (1909), S. 1641-1642 
    Details
    ISSN: 0044-8249
    Keywords: Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/ange.19090223305
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  • 6
    Electronic Resource
    Electronic Resource
    Beiträge zur Chemie des Phosphors. 144. Synthese und Eigenschaften des Hexaphospha-3-germaspiro[2.4]heptans (t-BuP)2Ge(t-BuP)4Professor Gerhard Fritz zum 65. Geburtstage am 14. Dezember 1984 gewidmet (1984)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 519 (1984), S. 24-30 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Contributions to the Chemistry of Phosphorus. 144. Synthesis and Properties of the Hexaphospha-3-germaspiro[2.4]heptane (t-BuP)2Ge(t-BuP)4The cyclocondensation of K(t-Bu)P—P(t-Bu)K with germanium tetrachloride in the molar ratio of 2:1 yields the novel spirocyclic compound 1,2,4,5,6,7-hexa-tert-butyl-1,2,4,5,6,7-hexaphospha-3-germaspiro[2.4]heptane, (t-BuP)2Ge(t-BuP)4 (1). Besides considerable amounts of (t-BuP)4 are formed and occasionally some (t-BuP)3 can be found. 1 could be isolated in the pure state and has been NMR-spectroscopically characterized as a spirocyclic compound with a P2GeP4 skeleton.
    Notes: Bei der Cyclokondensation von K(t-Bu)P—P(t-Bu)K mit Germaniumtetrachlorid im Molverhältnis 2:1 wird die neue Spiroverbindung 1,2,4,5,6,7-Hexa-tert-butyl-1,2,4,5,6,7-hexaphospha-3-germaspiro[2.4]heptan, (t-BuP)2Ge(t-BuP)4 (1), gebildet. Daneben entstehen beträchtliche Mengen an (t-BuP)4 sowie gelegentlich etwas (t-BuP)3. Verbindung 1 konnte in reiner Form isoliert und kernresonanzspektroskopisch als Spirocyclus mit P2GeP4-Ringgerüst charkterisiert werden.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19845191203
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