ISSN:
0044-2313
Keywords:
Chemistry
;
Inorganic Chemistry
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Description / Table of Contents:
Crystal and Molecular Structure, of S4N4 · 2C7H8The structure of the title compound has been determined from threedimensional X-ray data. Crystals are monoclinic, with unit cell dimenions a = 16.532 Å, b = 8.563 Å, c = 10.880 Å, β = 103.2°, space group C2h6—C2/c and Z = 4. Least squares refinement, by use of 1132 independent reflections measured on a diffractometer has reached 3.9%.In the S4N4·2C7H8 molecules the organic components are linked to two sulfur atoms of the S4N4, ring each.
Notes:
Die Struktur von S4N4 · 2C7H8 wurde röntgenographisch bestimmt. Die Verbindung kristallisiert monoklin, in der Raumgruppe C2h6—C2/c, mit a = 16,532 Å, b = 8,563 Å, c = 10,880 Å, β = 103,2° und Z = 4. Die Verfeinerung nach der Methode der kleinsten Quadrate ergab einen R-Wert von 3,9%.Die beiden Bicyclopentadien-Molekeln sind an je 2 Schwefelatome des S4N4-Ringes gebunden.
Additional Material:
1 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/zaac.19764200208
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