ISSN:
0749-1581
Keywords:
2D heteronuclear multiple-quantum NMR
;
Group assignment
;
13C and 1H shift measurements
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
A two-dimensional heteronuclear multiple-quantum NMR experiment, based on the DEPT pulse sequence, for the simultaneous determination of the nature of proton-bearing chemical groups together with the measurement and correlation of carbon and proton chemical shifts is presented. Time and computer memory requirements for the proposed experiment are comparable to the acquisition of a two-dimensional C,H shift correlation spectrum. The data evaluation of the proposed zero-quantum carbon-shift correlated spectrum provides a list of chemical groups corroborated with their carbon and proton chemical shifts.
Additional Material:
5 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260250117
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