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  • 1
    Electronic Resource
    Electronic Resource
    Titanocene Complexes Based on Benzenehexathiolate Derivatives and 2,3,6,7-Tetrachloronaphthalenetetrathiolate (1995)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 128 (1995), S. 1047-1049 
    Details
    ISSN: 0009-2940
    Keywords: (Dithiolato)titanocene complexes ; Sodium benzenehexathiolate ; Tetrabutylammonium 2,3,6,7-tetrachloro-5,8-dimercaptonaphthalenedithiolate ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The synthesis and properties of the new (dithiolato)titanocene complexes 4a-d, 6, 9 are described. The ligands of these complexes are derived from sodium benzenehexathiolate or 3,4,7,8-tetrachloronaphthobis[1,2]dithiole. Complexes with one, two and three (dithiolato)titanocene units were prepared by use of these dithiolato ligands.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19951281014
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    An Efficient Method for Synthesizing Substituted Naphtho-1,3-dithiole-2-thiones from Tetrachlorotetrathionaphthalene and Sodium Trithiocarbonate (1998)
    Weinheim : Wiley-Blackwell
    Liebigs Annalen 1998 (1998), S. 1577-1581 
    Details
    ISSN: 1434-193X
    Keywords: Sulfur heterocycles ; Synthetic methods ; Conducting materials ; Desulfurization ; C-C coupling ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Two types of naphtho-fused 1,3-dithiole-2-thiones (2a-f and 4a-d) were obtained by the reaction of 3,4,7,8-tetrachloro-naphtho[1,8-cd:5,6-c′d′]bis(1,2-dithiole) (1) and sodium trithiocarbonate. The dechalcogenization of the thiones, using mercury acetate, leads to the corresponding naphtho-1,3-dithiol-2-ones (3a-d and 5a-d). The structures of 3a and 4a were confirmed by X-ray investigation. The tetrathiafulvalenes (TTFs) 6 and 7 were synthesized from 2d and 3c by coupling of the starting compounds with the help of triethyl phosphite. Using 2,3-dichloro-5,6-dicyano-benzoquinone (DDQ) the TTFs were converted into semiconducting charge-transfer complexes.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
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