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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Advanced materials research Vol. 26-28 (Oct. 2007), p. 213-216 
    ISSN: 1662-8985
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The crystallographic orientation distribution, and its change as a function of creepdeformation in Ni-based single crystal superalloys have been investigated by X-ray diffractometry.The distribution of the crystallographic orientation has significantly broadened by creepdeformations. Directional broadening of the distribution agrees with creep dislocations having theburgers vector of 1/2〈101〉. High temperature creep strain of superalloys can be estimated by anon-destractive test where the width of rocking curve of a diffraction peak is measured
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 519-521 (July 2006), p. 1479-1484 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The effect of extrusion rate and ratio on the Al3Zr induced dynamic recrystallization(DRX) that occurs during hot extrusion of RS-P/M Al-Zn-Mg-Cu-Zr alloys was investigated. Anincrease in the logarithm of extrusion rate promoted DRX and lead to a monotonic increase in thenumber of fine grains. Although DRX was also promoted and the grain size reduced by an increase inextrusion ratio from 10 to 20, the DRX behavior hardly changed, even when the extrusion ratioexceeded 20. However, with increasing extrusion ratio, the width of fibrous grain, i.e., theunrecrystallized region, decreased and the tensile strength increased to 879 MPa.When the extrusion rate and ratio exceeded 54 mm/min and 20, respectively, a marked graincoarsening occurred upon solution treatment, and the tensile strength tended to decrease, because ofthe high dislocation density induced by hot extrusion. By annealing at 563 K before solutiontreatment, it was possible to prevent grain coarsening, and thus prevent the strength decrease
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 519-521 (July 2006), p. 1623-1628 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The Mesoalite alloy is formed using rapidly solidified powder metallurgy (RS-P/M) byhot extruding the RS powder produced by the atomization method. Meso20 is a Mesoalite alloy witha chemical composition of Al-9.5Zn3Mg-1.5Cu-4Mn-0.04Ag (mass%). Meso20 contains fine grainsand precipitated intermetallic Mn compounds, and has a tensile strength of 910 MPa. During hotextrusion, dynamic recrystallization occurs and the fine grains develop.During heat treatment of Meso20, rod-like and granular Mn intermetallic compounds precipitate.The rod-like compounds are about 1 Ìm in length and the granular compounds are about 1 Ìm indiameter. X-ray diffraction measurement, transmission electron microscopy and energy dispersiveX-ray (TEM/EDX) analysis and Rietveld analysis revealed the chemical composition of the granularand rod-like Mn intermetallic precipitates to be 86.5Al-10.9Mn-0.4Cu-0.9Zn-1.3Mg and 80.5Al -10.3Mn-4.2Cu-2.5Zn-2.5Mg (mass%), respectively. The granular and rod-like compounds wereidentified as the Al6Mn and Q phases, respectively, with both belonging to the space group Cmcm.The lattice constants of Al6Mn were a=0.754 nm, b=0.648 nm c=0.855 nm and those of the Q phasewere a=0.765 nm b=2.34 nm c=1.25 nm.Meso10, with a chemical composition of Al-9.5Zn-3Mg-1.5Cu-0.04Ag (mass%), contains no Mnand does not have fine grains, but rather coarse fibrous grains elongated along the extrusion direction.Thus the Mn intermetallic precipitates in Meso20 clearly affect the formation of fine grains.Microstructure development was studied during hot extrusion by observation using high resolutionElectron Back Scattering Pattern method. Fine grains were found to develop in areas, which wererelatively abundant in granular Mn intermetallic precipitates
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 519-521 (July 2006), p. 419-424 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: In order to improve the high-temperature strength of an Al-Cu-Mg alloy, Mn was added atsupersaturation to form a high-density dispersion of an intermetallic phase. In the P/M Al-3.6Mn-6.4Cu-3.6Zn-1.7Mg alloy (mass%), rod-like Al-Mn-Cu-Zn quaternary intermetallic phases (Q phase)several hundred nanometers in length were dispersed in the matrix. The chemical composition of theQ phase was determined by TEM/EDX to be 78.8Al-12Mn-8Cu-1.2Zn (at%). The crystal system,space group, and lattice parameters of the unit cell were identified to be orthorhombic, Cmcm and a =0.76, b = 2.11, c = 1.25 nm, respectively, by Rietveld analysis. Since the matrix of the alloy obtainedwas of the Al-Cu-Mg-(Zn) system, age-hardening occurred by formation of a GPB zone at roomtemperature and 448 K. At the peak level of age-hardening at room temperature, the tensile strengthat room temperature was 704 MPa, and the elongations were 8.0%. The high temperature strengths at523 and 573 K were 319 and 141 MPa, respectively, and the elongations were 17 and 34%,respectively
    Type of Medium: Electronic Resource
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