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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : International Union of Crystallography (IUCr)
    Acta crystallographica 35 (1979), S. 497-499 
    ISSN: 1600-5724
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Notes: The information content of so-called 'unobserved', or 'non-significant' reflexions obtained by diffractometer measurements has been experimentally studied, using data and input parameters for three previously deter- mined crystal structures. It can be concluded that even those reflexions having the largest σ(I)/I values contain significant information about both thermal and positional atomic parameters. It has been possible to carry out an acceptable refinement of one structure on the basis of only the set of structure factors discarded by the original investigator. Inclusion of the weakest reflexions in the refinements lowers the standard deviations, and so should be standard practice.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : International Union of Crystallography (IUCr)
    Acta crystallographica 34 (1978), S. 399-404 
    ISSN: 1600-5724
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Notes: The crystal structure of Cu9Al4 has been refined on the basis of 114 independent structure factors, averaged from a set of 2416 intensity measurements with a diffractometer on a spherical crystal of 0.05 mm diameter. Graphite-monochromatized Cu Kα radiation was used. The final R value was 2.4% when corrections for absorption and extinction had been applied. Anisotropic thermal parameters were introduced and shown to be significant. The occurrence of coherently scattering antiphase domains was found to be less than I%. All equivalent reflections and Friedel pairs were recorded with graphite-monochromatized Mo Kα radiation for ten selected index combinations. Observed and calculated anomalous dispersion effects were found to match closely, indicating that incoherent twinning was also practically non-existent.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Amsterdam : Elsevier
    Accident Analysis and Prevention 13 (1981), S. 11-16 
    ISSN: 0001-4575
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Architecture, Civil Engineering, Surveying , Psychology
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 67 (1990), S. 4238-4240 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A theoretical analysis of the origin of residual stresses in amorphous wires and their effect on the magnetostrictive properties has been made. The residual stress distribution (compression in the surface and tension in the center) in the wire is attributed to the different cooling rates experienced during solidification by different regions of the wire. Theoretically calculated results agree well with reported experimental data obtained from magnetic measurements.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 11 (1978), S. 148-150 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Spherical crystals of alloy phases too hard and brittle for grinding can be obtained by partial remelting and solidification of a powder sample. The alloy powder is blown through an argon-plasma jet melting the surface material of individual fragments, which solidify again as nearly perfect spheres. The yield is a mixture of different materials in which it is possible, however, after heat treatment to find good single crystals of the original composition. Spherical single crystals of Cu9Al4 have been produced by this method and used for a high-precision X-ray investigation described elsewhere.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 8 (1989), S. 122-124 
    ISSN: 1573-4811
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Acta crystallographica 36 (1980), S. 2220-2223 
    ISSN: 1600-5740
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Acta crystallographica 36 (1980), S. 527-532 
    ISSN: 1600-5740
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 26 (1991), S. 3951-3954 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract A Cu92.5Nb5Sn2.5 alloy has been rapidly quenched into a powder by ultrasonic gas atomization. The structure of the powder consists of finely dispersed Nb particles in a Cu-Sn matrix. The powder has been consolidated by hot extrusion at 650°C. The extrusion does not change the phases present in the material appreciably but annealing for 100 h at 650°C causes a transformation of the Nb particles to Nb3Sn. The extruded material shows superconductivity. The critical temperatureT c, of the asquenched alloys is 8.0 K but increases to 15.6 K after annealing for 100 h at 923 K. The upper critical magnetic field, $$H_{C_2 } $$ , and critical current density,J c, were 3.4 kOe at 4.2 K and 7.4×105 Am−2 at zero applied field and 4.2 K, respectively. The appearance of superconductivity is attributed to the proximity effect of the Nb3Sn phase particles which are sufficiently well distributed to satisfy the leak distance and the critical particle size.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 26 (1991), S. 963-969 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract The microstructure of rapidly solidified 65Al-20Cu-15Fe (at. %) powders was investigated by analytical transmission electron microscopy. It was found that segregation in the powder particle occurred during solidification. The major phase present in the powder particles was the icosahedral quasicrystalline l-phase, which was determined to have space group $$\bar 3\bar 5$$ . Two other crystalline phases, β-AlCu3 and θ-Al13Fe4, coexisted with the l-phase. The l-phase was revealed by convergent beam electron diffraction to have three-dimensional quasiperiodicity (τ = 1.618) which is different from quasicrystals in the other systems. The compositions of the three phases have been analysed by energy dispersive X-ray analysis. The l-phase in this system could be approximately described as Al5CuFe. The composition of the θ-Al13Fe4 was very close to the equilibrium condition while β-AlCu3 was far from stoichiometry. An orientation relationship between β-AlCu3 and θ-Al13Fe4 was found as follows: [110]β∥[010]θ [111]β∥[001]θ
    Type of Medium: Electronic Resource
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