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Chiral Separation of Carboxymethyl Derivatives of Amines by Liquid Chromatography on Reversed-phase Silica Gel Coated with N-n-Dodecyl-L-hydroxyproline (1999)

Yamazaki, Shigeo ; Ban'i, Keiko ; Tanimura, Takenori

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 22 (1999), S. 487-489

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ISSN: 0935-6304

Keywords: Carboxymethyl derivatives of amines ; dodecyl-L-hydroxyproline ; chelate ring ; chemiluminescence ; ruthenium complex ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: ---Carboxymethyl derivatives of amines containing a chiral α-carbon were separated into enantiomers by high-performance liquid chromatography using octadecylsilanized silica gel coated with N-n-dodecyl-L-hydroxyproline as the stationary phase and an aqueous solution containing copper(II) as the mobile phase. Detection was by post-column reaction involving derivatization to tertiary amine and chemiluminescence reaction of ruthenium bipyridine complex.

Additional Material: 3 Ill.

Type of Medium: Electronic Resource

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