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  • 1
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 85 (2002), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: High-strength porous alumina has been fabricated with a microstructure control using the pulse electric current sintering (PECS) technique. During sintering the discharge, which is assumed to take place in the voids between the particles, is thought to promote the bridging of particles by neck growth in the initial stages of sintering, leaving high porosity. The effect of dopants (MgO, 200 ppm; TiO2, 1000 ppm) and of secondary inclusions (3 vol% 3Y-TZP) on the constrained densification and the improvement in the mechanical behavior of porous alumina ceramics has been reported. The porosity of the fabricated porous alumina was controllable between 30% and 50% depending on the sintering temperature. The flexural strength of alumina having 30% and 42% porosity showed impressive values of 250 and 177 MPa, respectively. The dominance of the preferential neck growth of grains over densification significantly improved the mechanical properties of porous alumina, besides leaving high porosity.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 29 (1994), S. 250-254 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract A detailed microstructural analysis of slip-cast Si3N4/SiC-whisker composites has been made by TEM. In spite of the gentle forming process, SiC whisker breakage constitutes a fundamental feature of this material. The breaking takes place during the sintering process and could be associated with residual thermal stresses, as revealed by the experimental evidence. The dramatic decrease in the whiskers aspect ratio translates into little or no effect of whisker addition on the mechanical properties of the Si3N4 matrix.
    Type of Medium: Electronic Resource
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  • 3
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Reaction-bonded aluminium niobate-based composites with tailored microstructures were fabricated through controlled nucleation and growth of AlNbO4 needle-like grains. Using heating rates of 0.5 to 〈 160 °C min−1, the effects of heat-up period on microstructure development, and the volume content, grain-size distribution as well as aspect ratio of AlNbO4 grains has been investigated. The morphology of the final microstructure is principally determined by the grain growth during heat-up. Equiaxed to elongated grains were obtained by using different heating rates and thermal ageing at 1320 °C in air. SEM observations revealed that increasing the heating rate promotes the development of large and homogeneously distributed needle-like grains. The results presented show that tailoring of final AlNbO4 microstructures become possible by the control of heating rate.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 18 (1999), S. 865-867 
    ISSN: 1573-4811
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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