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  • 1
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: C/SiC composites were prepared via isothermal chemical vapor infiltration (ICVI). A novel process of in situ whisker growing and matrix filling during ICVI was devised to reduce the porosity of the C/SiC composites, by alternating the dilute-gas species. C/SiC composites with increased density were prepared successfully using this novel process, in comparison with those obtained from the conventional ICVI process. The whiskers seem to have grown into the large pores and modified the pore structure that is filled by the SiC matrix.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: We fabricated by metal organic deposition (MOD) using trifluoroacetic acid (TFA) via the“211 process”, and then evaluated the phase formation, texture evolution, and critical properties as afunction of the firing temperature and film thickness. In the fabrication process, Y2Ba1Cu1Ox andBa3Cu5O8 powders were used as precursors instead of Y-, Ba- and Cu-based acetates. The films werefired in the temperature range of 750°C -800°C and the film thickness of films was controlled byrepeating the number of coating cycles. The microstructure varied significantly with the firingtemperature. The grains size increased, the film became denser, and the degree of the texture andphase purity varied with increasing firing temperature. The films fired at 775°C after calcining at4005 showed the highest critical current (Ic) of 18 A/cm-width, which corresponds to a criticalcurrent density (Jc) of 0.9 MA/cm2. For multi-coated films, the Ic increased from 18 in the singlycoated film to 100 A/cm-width with the triply coated film. In contrast, the corresponding Jc were inthe range of 0.9-1.2 MA/cm2. Both Ic and Jc values decreased as the coating number repeated furtheras a result of the degraded microstructure
    Type of Medium: Electronic Resource
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  • 3
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: We fabricated Bi-2212/SrSO4 composite superconductors by the melt casting process andevaluated the effects of the powder mixing method and melting temperature on their microstructureand superconducting properties. In the melt casting process, the Bi-2212 powders were mixed withSrSO4 by hand-mixing (HM) and planetary ball milling (PBM) and then the powder mixtures weremelted at 1100℃~1200℃, solidified, and annealed.We found that the powder mixture prepared by PBM was finer and more homogeneously mixedthan that prepared by HM, resulting in more homogeneous microstructure and smaller SrSO4 andsecond phases after annealing. The critical current (Ic) also varied significantly with the powdermixing method and the melting temperature. The Ic of the annealed rod prepared by PBM was 193A at 77 K when melted at 1100℃, which is higher than that of the annealed rod prepared by HM(132 A). This enhancement in the Ic value for the former is considered to be due to its more uniformmicrostructure
    Type of Medium: Electronic Resource
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  • 4
    ISSN: 1573-4811
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 16 (1997), S. 80-82 
    ISSN: 1573-4811
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 18 (1983), S. 271-277 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Hydrogen trapping phenomena in carbon steel with controlled amounts of trapping site were studied by permeation experiments. The amount of hydrogen passed through carbon steel membranes was measured by gas chromatography and the diffusivities were calculated from permeation time-lag data. The permeability and diffusivity of hydrogen in carbon steel decrease as the ferrite-cementite interfacial area increases. The trap binding energy of the ferrite-cementite interfaces and hydrogen is calculated to be 10.85 kJ mol−1 and the energy level of hydrogen around the trap sites is estimated.
    Type of Medium: Electronic Resource
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  • 7
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Indentation-induced damage is investigated in silicon carbide (SiC) deposited on graphite substrate. The SiC films have been grown by LPCVD (Low Pressure Chemical Vapor Deposition) method using MTS (CH3SiCl3) as a source gas and H2 as a diluent gas to provide highly dense deposited layer and strong interfacial bonding. The elastic-plastic mismatch is very high to induce distinctive damages in the coating and the substrate layer. The specimens with various coating thicknesses are prepared by changing CVD condition or mechanical polishing. Indentation damages with different sizes are introduced by controlling indentation load in Nanoindentation, Vickers indentation and Hertzian indentation test. Basic mechanical properties such as hardness, toughness, elastic modulus are evaluated against coating thickness. Mechanical properties are sensitive to the indentation load and coating thickness. The results indicate that coating thickness has a vital importance on the design of hard coating/soft substrate system because the soft substrate affects on the mechanical properties.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 35 (2000), S. 4519-4526 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Silicon carbide films have been grown onto graphite substrates by low pressure chemical vapor deposition using MTS (CH3SiCl3) as a source precursor and H2 or N2 as a diluent gas. The experiments were performed at fixed conditions of a flow rate of 100 sccm for each MTS and carrier gas, a flow rate of 300 sccm for diluent gas addition, and a total pressure of 5 torr. The effect of temperature from 900°C to 1350°C and the alteration of diluent gas species on the growth rate and structure of deposits have been studied. The experimental results showed that the deposition rate increased with increasing deposition temperature irrespective of diluent gases and reactant depletion effect increased especially at H2 diluent gas ambient. At MTS-H2 system, the deposition mechanism changed from chemical reaction to mass transfer controlled reaction with temperature. Otherwise, For MTS-H2-N2 system, surface chemical reaction controlled the growth process at whole deposition temperature ranges. For N2 addition, surface morphology of leaf-like structure appeared, and for H2, faceted structure at 1350°C. The observed features were involved by crystalline phase of β-SiC and surface composition with different gas ambient.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 32 (1997), S. 4701-4709 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Crystallographic orientations of the Y211 tracks that were trapped within the melt-textured Y123 domains were determined from the orientation relationship among the Y211 pattern, $$\left\langle {110} \right\rangle $$ twin traces and a microcrack. Analysing the orientation of the two-dimensional Y211 patterns that were observed on various crystallographic planes of the Y123, the three-dimensional shape of the Y211 pattern was inferred as follows: only one x-type Y211 pattern was included within one Y123 domain and three sets of diagonal Y211 tracks met with the corners of the Y123 domain. The diagonal Y211 tracks lie on the (1 1 0), ( $$\bar 1$$ 1 0), (0 1 1), (0 $$\bar 1$$ 1), (1 0 1) and (1 0 $$\bar 1$$ ) planes of the Y123 domain. The planes where the Y211 tracks are located are considered to be the boundary planes where local growing parts of the Y123 domain impinge upon each other. The formation mechanism of the Y211 pattern is discussed on the basis of anisotropic growth behaviour and the shape of the Y123 domain.
    Type of Medium: Electronic Resource
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  • 10
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract YBa2Cu3O7-δ (Y123)-Ag composite superconducting wires were fabricated by the plastic extrusion method which involves plastic paste making, die extrusion, binder burn-out and the firing process. The as-extruded Y123-Ag wires were so flexible that they can be easily fabricated into a desirable shape. The current-carrying properties of the wire are dependent on sample size, sintering temperature and silver content. The critical current density, Jc, of the Y123 wire with a large cross-section was lower than that of the wires with a small cross-section, probably due to the large self-induced magnetic field. Jc of the Y123-Ag wires increased with increasing sintering temperature but abruptly decreased above 910°C, which is close to the eutectic temperature of the Y–Ba–Cu–O system. A silver addition of 10–20 wt% slightly increased Jc of the Y123 (at 77 K and 0 T, it was 140 and 250 A cm-2 for the undoped Y123 wire and the Y123 wire with 20 wt% Ag addition, respectively), but further silver addition had a deleterious effect on Jc (180 A cm-2 for 30 wt% Ag addition). The small increment in Jc in the Y123 wire with 10–20 wt% Ag addition appears to be due to the enhanced densification and the associated microstructural variation. The decreased Jc of the Y123 wire with 30 wt% Ag addition is considered to be due to the formation of non-superconducting phase, Y2BaCuO5 (Y211), BaCuO2 and CuO phases via the decomposition of the Y123 phase.
    Type of Medium: Electronic Resource
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