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  • 1
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 85 (2002), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Densification behavior of precursor-derived Si-C-N ceramics by hot isostatic pressing (HIP) has been investigated to obtain dense ceramics derived from polymer precursor. An as-pyrolyzed ceramic monolith, which had a porosity of about 17%, could be deformed up to a strain of 8% in preliminary uniaxial compression tests. The flow stress of the material was much higher than 200 MPa at 1600°C; thus high stress was necessary for densification by HIP. The density of the monolith increased from 1.9 to 2.4 g/cm3 by HIP at 1600°C and 980 MPa. Although the number of pores decreased, large pores were formed in the hot isostatically pressed monolith. On the other hand, denser ceramics, in which pores were not observed by optical microscopy, were obtained by hot isostatically pressing the pyrolyzed powder compact.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 317-318 (Aug. 2006), p. 15-18 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Consolidation of pyrolyzed powders has been tried by hot isostatic pressing (HIP) withoutsintering additives, in order to obtain dense non-oxide ceramic bulk materials derived from polymerprecursors. Si1.0C1.6N1.3 ceramic powders were derived from a polyvinylsilazane polymer. Thepolymer was thermally crosslinked at 250oC and pyrolyzed at 1050oC under Ar atmosphere. Thepyrolyzed powders were die-pressed into rectangular bars at room temperature and densified by HIPat 1400oC-900 MPa and 1500oC-950 MPa. Dense ceramic monolith, in which pores were notobserved by optical microscopy, was obtained by the HIP consolidation at 1500oC-950 MPa. Themicrostructure of the ceramic monolith was a nano-composite structure consisted of α-Si3N4 andgraphite phases. In the compression tests of the HIP-treated sample, slight plastic deformation wasobserved at 1400 and 1500oC in spite of high compressive stress over 1000 MPa. On the other hand,the sample showed a compressive strain of about 7% at 1000 MPa at 1600oC. The compressive strainof about 11% was achieved at 1700oC
    Type of Medium: Electronic Resource
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