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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 308-311 (May 1999), p. 766-773 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 299-300 (Dec. 1998), p. 165-170 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 3
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    Journal of thermal analysis and calorimetry 33 (1988), S. 559-565 
    ISSN: 1572-8943
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zusammenfassung Beim Sintern vielkomponentiger Systeme, die aus Gemischen der Komponenten hergestellt werden, bestimmt eine Vielzahl von Festkörperreaktionen, Neubildung und Auflösung von Phasen und das Auftreten von flüssigen Phasen die Verdichtung und die erreichbare Mikrostruktur des Materials. Ergebnisse der Untersuchung in den Systemen WC-Co und Fe-Si durch kombinierten Einsatz von Dilatometrie, TG-DTA, metallographischen und Mikrosonden-Untersuchungen werden mitgeteilt.
    Abstract: Резюме В процессе спекания м ногокомпонентных си стем, полученных с помощью твердотельных реакций смеси компон ентов, образование фа зы или растворение, также ка к и наличие жидкой фазы определя ют плотность и конечн ую микроструктуру мате риала. Представлены результаты исследов аний систем WC-Со и Fe-Si с использованием мето дов дилатометрии, дифференциального т ермического анализа и термогравиметрии, со пряженных с металлографическим анализом и анализом м икропробы.
    Notes: Abstract During the sintering of multicomponent disperse systems prepared from mixtures of the components, a variety of solid-state reactions, phase formation or dissolution, and the occurrence of a liquid phase determine the densification and the final microstructure of the material. The results are presented of investigations on the systems WC-Co and Fe-Si, through the simultaneous application of dilatometry, differential thermal analysis and thermogravimetry, coupled with metallographic and microprobe analysis.
    Type of Medium: Electronic Resource
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  • 5
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract We consider the specific problem of the influence of an inhomogeneous distribution of defects in solids on positron annihilation characteristics. In detail, we investigate the effect of micro-structure, i.e. dislocations, vacancies, vacancy clusters, grain and subgrain boundaries, pores or inner surfaces, on positron lifetime spectroscopy. Only few materials show such small grain sizes that positron annihilation is affected. One example are powder compacts, made out of small and fine-grained powder, during different stages of the sintering process. All samples generically show positron trapping at grain boundaries (τGB ≈ 300 ps) and at surfaces (τsurf = 500–600 ps). τGB = 300 ps corresponds to small voids consisting of roughly eight vacancies. Different defects can lead to similar annihilation parameters. Hence, we compare the lifetime data obtained from porous and fine-grained samples to the kinetics of defect annealing after irradiation and plastic deformation, e.g. the thermal stability of dislocations or vacancy clusters. We conclude that τGB ≈ 300 ps is apparently not related to vacancy clusters in the matrix, but is due to positron trapping at large-angle grain boundaries. This large open volume is in contrast to common grain boundary models. The change of porosity and grain size with temperature, i.e. during sintering, has been determined in a correlated study by metallography and X-ray line-profile analysis. The effective powder particle size ranges from ≈0.5 to ≈15 μm, while the grain sizes are always smaller. The only detectable lattice defects in all samples above recrystallization temperature are grain boundaries, besides a surface component in very fine powders.
    Type of Medium: Electronic Resource
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