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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 138 (Mar. 2008), p. 175-180 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: Lightweight B4C/Al composites were produced from powders of boron carbide andaluminum by self-propagating high-temperature synthesis (SHS). The effects of postdensificationheat treatment at different temperatures and environmental conditions on phase transformations andproperties evolution were studied. Heat treatment processing that followed the synthesis was appliedusing low heating rate in temperature range from 400°C up to 1500°C. An interconnectedmultiphase (B4C, Al3BC, and c-BN) microstructure was produced in composite as a result of heattreatment at temperatures below 1080°C. The formation of hard and brittle reaction products (AlN,AlB2, Al4C3, and Al8B4C7) at temperatures above 1150°C causes decrease in bending strength andincrease in resistance to unlubricated sliding wear
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 584-586 (June 2008), p. 349-354 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: High purity (99.99, wt %) niobium ingots were received by double electron beam meltingtechnology. The specimens of pure metals with cast microstructure were processed using coldequal-channel angular pressing (ECAP) followed by a heat treatment at around 1080 °C in vacuumfurnace for 2 h. Shear bands and microstructure evolution was studied in shear region at first passand at next passes of ECAP. Microstructure processing characterization was performed using lightoptical and field emission scanning electron microscopy. Accompanied to microstructure thechanges of mechanical properties were determined by micro- and universal hardness testing. Theshear bands forming, evolution of large crystals to elongated laminar and dislocation fine-grainstructures during processing was characterized and discussed in view of metal hardening-softeningand viscoplastic behavior under subsequent hard cyclic straining
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 584-586 (June 2008), p. 361-366 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Annealed pure copper was subjected to equal-channel angular pressing (ECAP) by routeBc for different passes number. Tensile test specimens were manufactured and subjected to hardcyclic viscoplastic (HCV) deformation by means of the materials testing installation Instron 8516 instrain control regime at room temperature. The specimens were cyclically deformed with afrequency of 0.5Hz at different strain amplitudes, step-by-step increased from ±0.05 to ±2.5% for30 cycles, up to seven test series in this study.The microstructure of ECAP and HCV deformed samples were characterized by optical- andtransmission electron microscope, X-ray diffraction, tensile- and hardness testing methods.The ECAP processed metal has mainly elongated subgrains with low-angle grain boundaries andtexture, oriented in direction of metal flow during latest pressing. We demonstrate that during HCVdeformation the dislocations density of ECAP processed UFG copper was decreased. The ECAPtexture was reoriented under cyclic load applied as elongated subgrains were jointed to small piecesunder this same angle to axis as texture before. The grain- and crystallite sizes were decreased,which were accompanied with dislocation ribbons forming nearby new formed high-angle grainboundaries. This paper builds on knowledge that the combined treatment by ECAP and followedHCV deformation enable to improve UFG microstructure and ductility with lowering the strengthand hardness of UFG metals due to the lower dislocation density while coarse grained copperexhibits increasing the strength and hardness
    Type of Medium: Electronic Resource
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