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  • 1
    Electronic Resource
    Electronic Resource
    s.l. : American Chemical Society
    Industrial and engineering chemistry 7 (1968), S. 385-389 
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. : American Chemical Society
    Industrial and engineering chemistry 12 (1973), S. 300-305 
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 15 (1969), S. 4-10 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: A dye tracer technique was utilized to measure the residence time distribution of the drops in a spray column, operating with a dispersed or a dense packing of drops, for a wide range of flow rates, in a 15 cm.in diameter, 150 to 160 cm. long column proper.For dispersed packing of drops and for flow rates below the onset of coalescence, the flow of the drops was approximately plug flow, with a variance of the residence time distribution of 0.095. For flow rates above the onset of coalescence within the column, the variance increased sharply to 0.55 and decreased at higher flow rates.For dense packing of drops the variance of the residence time distribution was in the range of 0.1 to 0.5. This variance is attributed to the effect of bypassing water and kerosene near the wall of the column. A mathematical model based on this effect showed reasonable fit with the experimental results. This model predicts an approach to plug flow of the drops for large diameter columns.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 17 (1971), S. 867-872 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: No. Abstract.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 17 (1971), S. 984-990 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Extraction in spray columns is reexamined in view of recent information on wakes of drops and the role of wakes in the mechanism of heat transfer in spray columns. In the proposed mechanism, mass is extracted from a highly mixed drop to a highly mixed wake in the wake growth zone. Elements of wakes are shed, mixed with continuous phase, and are replaced by the continuous phase in the wake shedding zone. A narrow mixing zone exists at the entrance of the continuous phase and above it the coalescence zone.A mathematical model for extraction in spray columns is presented. This model was used to calculate the top concentrations from the bottom concentrations, for 258 runs from nine papers covering very wide ranges of columns, systems, and operation parameters. Better than 20% agreement was obtained for 10 runs and the poorer agreement of most other runs can be attributed to the sensitivity of the calculations to the uncertainties in the average distribution coefficients of the solute between the two liquid phases, and, to a lesser extent, to the uncertainties in the length of the wake shedding zone and wake parameters. For very large or very small values of the distribution coefficient, the assumption of local equilibrium between drop and wake, used in the model, does not hold.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 14 (1968), S. 831-833 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 11 (1965), S. 804-808 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Temperature profiles were measured in a spray-column heat exchanger 7.5 cm. in diameter and 167 cm. long between the inlets of warm kerosene and cold water. The temperature jump, at the inlet of the continuous phase, is a measure of the amount of mixing in the column and is a function of holdup and ratio of flow rates of the two phases. At holdup the temperature jump had a minimum value of 0.24.A physical model for heat transfer in a spray column based on hydrodynamic principles is proposed. Heat is transferred from drop to wake downstream of drop. Wakes are shed and mixed with the bulk water flow. New material enters the wake and is spilled out at higher temperatures.The physical model is applied to explain the data on temperature jumps in spray-column heat exchangers and the data on concentration jumps in spray-column extractors.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 14 (1968), S. 398-405 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Temperature profiles of dispersed kerosene and water were measured in a spray column heat exchanger, 15 cm. in diameter and 160 cm. long. Dispersed packing of drops and narrow temperature ranges were used. The flow rates used were 0 to 50 liters/min. of water and 5 to 40 liters/min. of kerosene. The physical picture that emerges from the temperature profiles is that heat is transferred from fully mixed drops to fully mixed wakes while the wakes are formed, by shedding and renewal of elements of wakes in most of the column and by complete mixing of all streams at the water inlet at the top of the column. Mathematical equations were developed from the physical model. The volume of the wakes and the rate of shedding of wake elements were estimated from the temperature profiles and were used to calculate the temperature profiles for this and for other studies. The agreement of the calculated profiles with the experimental data is very good.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 13 (1967), S. 443-449 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Local and average holdup and drop size distribution as function of flow rates were measured for kerosene drops and water in a countercurrent, 15-cm. I.D., 160-cm. long, spray column. The range of flow rates was 5 to 40 liters/min. of kerosene and 0 to 50 liters/min. of water. At the same pairs of flow rates of the dispersed and the continuous phases in spray columns, three modes of drop packings can be obtained. These are termed, in order of increasing average holdup and increasing regularity of flow patterns, dispersed, restrained, and dense packings. For dispersed packing, at low flow rates of the two phases, the holdup and the drop size are constant along the column. At high flow rates the drop size increases from bottom to top of the column and the holdup increases from top to bottom of the column. The range of flow rates for the operation of a spray column is extended by the use of a conical entry section (Elgin design) at the bottom of the column, by the formation of an equilibrium region in the conical section.The average holdup increases with increased flow rates of both phases for dispersed and restrained packings, and with decreased flow rates of both phases for dense packing.The best definitions of flooding in a spray column are either the point of maximum average specific area of the drops, which corresponds to the onset of coalescence in the column, or the start of rejection of drops from the column proper.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 16 (1970), S. 955-963 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Temperature profiles of water in a spray column heat exchanger, 15 cm. in diameter and 150 cm. long, operating with a dense packing of kerosene drops, were measured. The range of superficial velocities was 0 to 0.8 cm./sec. of water and 0.5 to 1.7 cm./sec. of kerosene. The bottom of the dense packing was either slightly above or 15 cm. below the bottom of the column proper.The physical picture of heat transfer is similar to that for dispersed packings of drops and emphasizes the dominant role of wakes in the heat transfer mechanism. The mathematical equations for dispersed packings of drops were modified to take into account the reduction of wake size at the interface of the two packings and the difference in the mixing patterns at the top of the column. An empirical allowance for the effect of bypassing is suggested. The volume of the wakes and the rate of wake shedding were estimated from the temperature profiles. General agreement was found between the theory and the experimental data of this and three other studies.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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