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Chemical ionization mass spectrum of peroxyacetylnitrate (1976)

Pate, Christopher T. ; Sprung, Jeremy L. ; Pitts, James N.

Chichester : Wiley-Blackwell

Biological Mass Spectrometry 11 (1976), S. 552-555

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ISSN: 0030-493X

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The chemical ionization mass spectrum of peroxyacetylnitrate, a major component of photochemical smog highly toxic to man and plants, was obtained using both methane and isobutane as reagent gas. The spectrum contains a [M + H]+ ion at m/e 122, intense fragment ions at m/e 43 [CH,CO]+ and m/e 46 [NO2]+, and less intense ions at m/e 61 [CH,ONO]+, m/e 77 [CH30NOz]+ and m/e 88 [+O≡CCH2ONO] formed by internal rearrangements. These results confirm the commonly accepted structure for peroxyacetylnitrate, CH3(CO)OONO2.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/oms.1210110514

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