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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 90 (2001), S. 456-461 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We investigated the relative merits and limits of pulsed laser deposition from AlN targets in vacuum and low-pressure nitrogen in obtaining stoichiometric and crystalline aluminum nitride thin films. We used two UV excimer laser sources (λ=248 nm): a nanosecond system (τFWHM=30 ns) and, a subpicosecond (τFWHM=450 fs) system. The obtained structures were characterized by x-ray diffraction, electron microscopy in cross section, selected area electron diffraction, and profilometry. We demonstrated that the best results are obtained with the sub-ps laser source in vacuum and in low pressure nitrogen when the AlN thin films are very pure, crystalline, clearly exhibiting a tendency to epitaxy. Metallic Al is present in the films deposited with the ns laser source. We believe this is an effect of the gradual decomposition of AlN inside the crater on the target surface under multipulse laser irradiation. © 2001 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: In this article, two original studies of the alumina as porous substrate and PLD (pulsed laserdeposition) thin films in view of its biomedical and tribological applications are presented.The first biomedical study aimed to evaluate the role of Al2O3 on thin deposited nanostructures. Forthis purpose, cerium stabilized zirconia doped hydroxyapatite thin films were deposited by PLDonto high purity, high density alumina substrates with different low porosities. For deposition, anUV KrF* (λ=248 nm, τ ~ 25 ns) excimer laser was used for the multi-pulse irradiation of the targets.The nanostructured surface morphologies of the thin films with micro droplets were evidenced byatomic force microscopy and scanning electron microscopy and the compositions with a Ca/P ratioof 1.7 by energy dispersive spectroscopy. The films were seeded with mesenchymal stem cells for invitro tests. The cells showed good attachment and spread and covered uniformly the surface of thesamples. Different functions of substrate porosities are observed in the efficiency of developing longfilopodia and of obtaining the optimal intracellular organization.The second study aimed to understand the influence of micro-structural and mechanicalcharacteristics on the tribological behaviour of stainless steel samples with PLD alumina coatingsproduced using an UV KrF* (λ=248 nm, τ ~ 20 ns) excimer laser and a sintered alumina target.Various microscopic observation techniques were used in order to connect the tribological responseto the amorphous microstructure of the coatings. The results correspond to the determination of themechanical characteristics by nanoindentation tests, scratch tests, and a tribological behaviouranalysis of the treated steel against 100Cr6. The films were stoichiometric, partially crystallizedwith an amorphous matrix and their surfaces had few particulates deposited on. The obtained valuesof hardness and elastic modulus of the films were in good agreements with literature data
    Type of Medium: Electronic Resource
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