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Investigations on the synthesis of Dimethylbenzodiazepinium Tetrahalogenometalate Complexes (1991)

Steinborn, Dirk ; Dung, Pham Gia ; Sedlak, Ursula

New York, NY : Wiley-Blackwell

Journal für Praktische Chemie/Chemiker-Zeitung 333 (1991), S. 327-332

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Details

ISSN: 0021-8383

Schlagwort(e): Chemistry ; Organic Chemistry

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: o-Phenylenediamine and acetylacetone react with MCl2 (M = Fe, Co) to give dimethylbenzodiazepinium tetrahalogenometalate complexes [dmb]2[MCl4]1, but in the presence of NiCl2 only [dmb]Cl is obtained. The complexes [dmb]2[MX4] (M = Fe, Co, Ni; X = Cl, Br) have been prepared by the reaction of MX2 with [dmb]X and in the case of nickel also by metathetical reaction of tetrahalogenoniccolat complexes with [dmb][BPh4]. All complexes described have been characterized by elemental analysis, magnetic measurement and spectroscopically.

Zusätzliches Material: 1 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/prac.19913330219

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