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  • 1
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A mostly single bcc phase with nanoscale grain sizes of 10 to 20 nm was found to form by annealing amorphous Fe-Zr-B, Fe-Hf-B, and Fe-M-B-Cu(M=Ti, Zr, Hf, Nb, and Ta) alloys for 3.6 ks in the range of 723 to 923 K. The high permeability (μe) above 10 000 at 1 kHz combined with high saturation magnetization (Bs) above 1.5 T was obtained for the bcc alloys. The highest μe and Bs values reach 14 000 and 1.7 T for Fe91Zr7B2, 20 000 and 1.55 T for Fe87Zr7B5Cu1, and 48 000 and 1.52 T for Fe86Zr7B6Cu1. Magnetostriction (λs) decreases significantly by the phase transition from amorphous to bcc phase and is measured to be 1 × 10−6 for the bcc Fe86Zr7B6Cu1 alloy. The small λs as well as the small grain size is concluded to be the reason for the good soft magnetic properties. The lattice parameter of this bcc phase is 0.2870 nm being larger than that of pure α-Fe. The small λs seems to be achieved by the dissolution of solute elements above an equilibrium solubility limit. The bcc Fe86Zr7B6Cu1 alloy also shows the low core loss of 0.066 W/kg at 1 T and 50 Hz, which is considerably smaller than that of amorphous Fe78Si9B13 and bcc Fe-3.5mass%Si alloys in practical uses as core materials in transformer.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 74 (1993), S. 3316-3322 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Magnetic core properties, core loss, permeability, and saturation magnetic induction of bcc-nanocrystalline Fe–M–B (M=Zr, Hf, and Nb) alloys produced by annealing a melt-spun amorphous phase were investigated in a ring-shaped form with the aim of clarifying the application potential as a core material. The bcc alloys exhibit high saturation induction (Bs) from 1.49 to 1.63 T combined with high permeability (μe) from 22 000 to 32 000 at 1 kHz and 0.4 A/m. The bcc Fe–M–B (M=Zr, Hf, or Nb) alloys also show low core losses (W) from 1.4×10−1 to 2.1×10−1 W/kg at 50 Hz and 1.4 T and from 1.70 to 2.50 W/kg at 1 kHz and 1.0 T. The W values attained for the bcc Fe–M–B (M=Zr, Hf, and Nb) alloys are smaller by 60%– 90% at 50 Hz and 1.4 T and 50%–70% at 1 kHz and 1.0 T, as compared with those for an amorphous Fe78Si9B13 alloy in practical use as a transformer core material. The low W values for the bcc-nanocrystalline alloys are presumably due to the small anomaly factor comparable to a Co-based amorphous alloy. The comparison of the present data with those for the amorphous Fe78Si9B13 alloy indicates that the bcc-nanocrystalline Fe–M–B (M=Zr, Hf, and Nb) alloys are promising for practical use as core materials.
    Type of Medium: Electronic Resource
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