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  • Electronic Resource  (18)
  • 1
    Electronic Resource
    Electronic Resource
    [s.l.] : Nature Publishing Group
    Nature 262 (1976), S. 613-615 
    ISSN: 1476-4687
    Source: Nature Archives 1869 - 2009
    Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics
    Notes: [Auszug] Unfortunately both structural signs can be faulted, the electron microscopy because of the possibility of fixation or postfixation changes6, and the X-ray diffraction because of the long time which was used to obtain the required exposures2,4. We have tried to overcome these objections by observing ...
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [s.l.] : Nature Publishing Group
    Nature 230 (1971), S. 434-437 
    ISSN: 1476-4687
    Source: Nature Archives 1869 - 2009
    Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics
    Notes: [Auszug] Some preliminary results have been obtained with synchrotron radiation from the 7.5 GeV electron synchrotron Deutsches Elektronen - Synchrotron (DESY) in Hamburg as a source for X-ray ...
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Palo Alto, Calif. : Annual Reviews
    Annual Review of Biophysics and Biomolecular Structure 5 (1976), S. 239-270 
    ISSN: 0084-6589
    Source: Annual Reviews Electronic Back Volume Collection 1932-2001ff
    Topics: Biology , Physics
    Type of Medium: Electronic Resource
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  • 4
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: An ultrahigh precision coupling of the angular motion of the two axes in a double-crystal monochromator with constant exit height has been constructed. The coupling device is a double parallelogram similar to the kind used for drafting tables. Computer simulations have been used to minimize the angular motion in the joints of the parallelograms to less than ±5° for the entire Bragg-angle range from 10° to 71°. This allows the use of backlash-free and friction-free flexural pivots. The axis of the first crystal is controlled by a precision rotary table. The shaft of the second crystal stage is supported by a trolley riding on a translation stage. Bearings allow for free rotation of the shaft. The double parallelogram provides only for the exact angular position of the second axis but does not support any weight of the second crystal stage and freely follows the trolley. The trolley is positioned so that the beam from the first crystal is intercepted and reflected at the correct height. The device is ultrahigh vacuum compatible. This design, which fully separates the two demands for extremely precise angular tracking and for less precise positioning for constant exit height, has several advantages beyond its superior tracking accuracy. The stationary first axis allows efficient, in-vacuum cooling of the first crystal. A direct rotary drive can be used for the first axis thus providing direct linear Bragg-angle control. A heavy weight second crystal stage, e.g., for sagittal focusing, may be used without deforming the angular linkage mechanism since all weight is carried by the rugged translation stage. No high-precision machining such as grinding or lapping is needed for the double-parallelogram linkage. The arms of the parallelogram, i.e., the distance between the holes for the flexural pivots, need to be only of precisely the same length.Testing the linkage shows the expected high accuracy. The maximum nonrepeatable deviation between the two axes is less than 5×10−5 degree (=0.2 arcsec). The tracking error for a 10−4 degree step is less than 1×10−5 degree, for a 10−3 degree step it is less than 2×10−5 degree. The maximum total deviation at any point within an interval of 0.1° is less than 1×10−4 degree (=0.4 arcsec). Repeatable and smooth long range deviations of a few arcseconds are compensated by feeding a predetermined corrective voltage to a piezo translator.
    Type of Medium: Electronic Resource
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  • 5
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A sagitally focusing stage has been constructed for the double-crystal scanning monochromator on beam line X9-A at the NSLS which can be exchanged with the normally used flat crystal stage. The bending device located at 12.0 m from the source is designed to accept a beam up to 200-mm wide. The monochromator with bending stage can be scanned over Bragg angles from 10° to 71° corresponding to photon energies from 11.4 to 2.1 keV with Si-111 crystals. In conjunction with the vertically focusing mirror a point focus of 0.38 mm×0.18 mm [horizontal×vertical, full width at half maximum (FWHM) each] has been achieved at a focal length of 3.8 m (center of a four-circle diffractometer). Focused at the back of the experimental hutch (focal length=5.4 m) the focal size was 0.55 mm×0.30 mm. The measured horizontal width of the focus equals the calculated size of the demagnified source and is independent of the horizontal convergence used. The horizontal focus produced by the crystal is very clean: the full width at 1% of maximum is 1.5 mm and at 0.01% it is about 4 mm. The flux into the focus is 5×1011 photons/s at a photon energy of 7.4 keV and beam current of 200 mA.The average flux density in the center of the focus (FWHM area) is 5×1011 photons/s/mm2. The preliminary crystal presently used has been made from a thin Si plate of 0.4-mm thickness, 80-mm width, and 75-mm length (in the direction of the beam). Steel ribs of 0.6-mm thickness have been glued at 3-mm pitch to the back of the crystal in order to stiffen the plate and reduce anticlastic bending.1 Plates have been glued to this crystal plate to extend the width to size the bending stage. The crystal was cut in 111 orientation with a 4° angle between the lattice planes and the crystal surface. The asymmetric cut was used to increase the angle of incidence and thus decrease the effect of the remaining anticlastic bending. The bending stage has a bending couple at both ends of the crystal in order to produce the desired curvature of the crystal. The bending couples can be adjusted to produce a conical shape as needed for the particular choice of focal length.2 Small piezotranslators push on the bending couples to remove small amounts of twist in the crystal introduced by alignment errors of the bending couples. All of the adjustment drives are outside of the monochromator tank and transmitted to the bending stage via linear feedthroughs and cables. A full description of this device and the crystal with glued ribs will be submitted shortly to this journal. This work was supported by Grant RR-01633, National Institutes of Health, Division of Research Resources.
    Type of Medium: Electronic Resource
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  • 6
    ISSN: 0196-9781
    Keywords: Arterial pressure ; Gastric acid ; Neuropeptide Y ; Pancreatic polypeptide ; Peptide YY
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Amsterdam : Elsevier
    Neuropsychologia 18 (1980), S. 185-191 
    ISSN: 0028-3932
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Psychology
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Amsterdam : Elsevier
    Nuclear Instruments and Methods 152 (1978), S. 191-194 
    ISSN: 0029-554X
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Energy, Environment Protection, Nuclear Power Engineering , Physics
    Type of Medium: Electronic Resource
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  • 9
    ISSN: 0029-554X
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Energy, Environment Protection, Nuclear Power Engineering , Physics
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Chester : International Union of Crystallography (IUCr)
    Journal of synchrotron radiation 7 (2000), S. 61-68 
    ISSN: 1600-5775
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: The Structural Biology Center beamline, 19ID, has been designed to take full advantage of the highly intense undulator radiation and very low source emittance available at the Advanced Photon Source. In order to keep the X-ray beam focused onto the pre-sample slits, a novel position-sensitive PIN diode array has been developed. The array consists of four PIN diodes positioned upstream of a 0.5 µm-thick metal foil placed in the X-ray beam. Using conventional difference-over-the-sum techniques, two-dimensional position information is obtained from the metal foil fluorescence. Because the full X-ray beam passes through the metal foil, the true beam center-of-mass is measured. The device is compact, inexpensive to construct, operates in a vacuum and has a working range of 8 mm × 10 mm that can be expanded with design modifications. Measured position sensitivity is 1–2 µm. Although optimized for use in the 5–25 keV energy range, the upper limit can be extended by changing metals or adjusting foil thickness.
    Type of Medium: Electronic Resource
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