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  • 2005-2009  (3)
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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 527-529 (Oct. 2006), p. 9-14 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The defect distribution in 4H-SiC single crystals in dependence on the seed polarity andits off-orientation was investigated by KOH-etching, optical microscopy and X-ray topography.Micropipe density, stacking fault density and dislocation density were determined for 2” crystalsgrown in 〈000-1〉 direction 0 - 7° off towards 〈11-20〉 and for crystals up to 1” in diameter grownin 〈11-20〉 or a- and 〈1-100〉 or m-directions and using repeated a-face growth. For the growth inpolar directions the micropipe density and dislocation density decrease with increasing offorientationof the seed. A similar behavior was found for the stacking fault density and dislocationdensity in non-polar directions with off-orientation to c-direction. Nevertheless, while thedislocation density could be reduced up to three orders of magnitude for the growth along non-polardirections, the stacking fault density was continuously increasing. Additionally, the defectdistribution after repeated a-face growth will be discussed in terms of growth related and kineticmodels
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 556-557 (Sept. 2007), p. 21-24 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: C-plane substrates with off-orientation to 〈1120 〉 may stabilize the grown polytype, butthe stacking fault density (SFD) increases from zero in the on-axis sample to 4500 cm-1 (7.7° off).The SF form preferentially at the seed-crystal-interface by a kinetically induced rearrangement ofsurface ad-atoms on m-facets. Most SF start in bundles with an average distance of 100 .m, whichare subdivided in smaller bundles with 8 .m distance. They start preferentially from the uppercorner of the vertical non-polar plane of bunched steps, which may be composed of small pyramidswith m-facet surfaces. The dislocation density could decrease with increasing SFD by a pinningmechanism
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 483-485 (May 2005), p. 39-42 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Planar defects have been found in nitrogen doped 2" 4H-SiC crystals grown on off-axis seeds. The doping level was 1×1019cm-3, which is below the critical one for the thermally activated cubic stacking fault formation in the 4H matrix. Planar defects in the doped region are nucleated on the whole seed surface outside the growth facet. They are coexisting 15R and 6H lamellas of unitcell height as revealed by means of luminescence and high resolution transmission electron microscopy. These inclusions are preferably formed at the rim of the growth facet, where polytype change occurs after switching off the nitrogen flow during growth
    Type of Medium: Electronic Resource
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