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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 5060-5062 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We have prepared nanometer-size, isolated CoPt particles. The particles in the range of 100–300 nm in diameter were formed by annealing thin films in the temperature range of 550–800 °C. Films with magnetic coercivity as high as 30 kOe were achieved. The results indicate that the high magnetic coercivity was obtained because the crystallite size approaches that of noninteracting single-domain particles. © 1996 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 5958-5960 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Rare earth–cobalt (RCo, R=Sm, Pr) films with thicknesses from 30 to 700 nm have been prepared with and without a Cr underlayer by dc magnetron sputtering from a R2Co7 composite target. The as-deposited SmCo films with a Cr underlayer (SmCo(parallel)Cr) have magnetic coercivities of about 500–2800 Oe and the PrCo(parallel)Cr films have coercivities of about 100–300 Oe, but after annealing at 500 °C coercivities as high as 31 kOe for SmCo(parallel)Cr films and 10 kOe for PrCo(parallel)Cr films were observed. The as-deposited PrCo films are composed mostly of an amorphous phase with about 30 vol % of crystallites but after annealing at 500 °C the film is transformed completely to crystallites of about 10 nm diameter as revealed by high-resolution transmission electron microscopy (HRTEM). Nanodiffraction and HRTEM studies show that the crystallites have a closed-packed hexagonal structure. HRTEM study also shows that the annealed SmCo films with a Cr underlayer have grain sizes of about 20 nm and the SmCo films without the Cr underlayer have grain sizes of about 10 nm. The large increase in coercivity for the annealed films is due to the growth of the crystallites. © 1996 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 6448-6450 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We report on magnetic force microscopy (MFM) images of a thin-film magnetic recording head taken using batch micromachined silicon tips coated with nanocomposite Fe60(SiO2)40 and Fe70(SiO2)30 films. The small Fe grain size (〈10 nm) and dilute Fe volume fraction (0.29–0.4) of these granular films produce tip coatings of low remanence and essentially zero coercivity, reduced by the superparamagnetic properties of these films. We have used these tips to obtain MFM images of the write field of the head with high spatial and magnetic-field resolution. In comparison to images taken using commercial Co85Cr15-coated tips, these MFM images show reduced tip memory effects and clearly delineate the gap field from the pole pieces. © 1996 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 77 (1995), S. 3831-3835 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Sm-Co film is a potential candidate for the future high density recording media of 10 Gb/in2 which requires bit sizes of the order of 300 nm and grain sizes of about 10 nm. This article investigates the microstructure of the Cr underlayer in Sm-Co thin films and its effect on Sm-Co thin films prepared by the dc magnetron sputtering technique. The grain size of the Cr underlayer is found to be about 25 nm. Grains with small angle misorientation usually form local agglomerates. Studies by transmission electron microscopy (TEM) bright field images at different defocus settings and by high resolution electron microscopy indicate that a large proportion of the grain boundaries have gaps. The gap width (about 1–3 nm) varies from place to place. The Sm-Co films deposited on the Cr underlayer inherit similar gaps at positions adjacent to the grain boundary gaps of the Cr underlayer. Such gaps produce grain-like contrast of about 25 nm in TEM bright field images. However, such contrast becomes weak as the thickness of the film increases and disappears at a thickness of 96 nm, suggesting the gaps are sealed at places far from the Cr underlayer. The effect of the Cr underlayer on magnetic properties are discussed. © 1995 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 85 (1999), S. 4334-4336 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: In this study, we showed that a magnetic coercivity (Hc) as high as 37 kOe was obtained in a CoPt thin film that contains separated nanometer-size CoPt crystallites. We prepared CoPt thin films with thicknesses of 5 and 175 nm by magnetron sputtering. After annealing in an Ar/H2 atmosphere at temperatures from 650 to 750 °C for 3–12 h, we measured the magnetic properties and found that magnetic Hc relates to annealing temperature, annealing time and film thickness. From atomic force microscopy and magnetic force microscopy studies, the magnetic single domain size of CoPt is in the range of 100–200 nm. The high Hc is likely due to the well-separated nanometer-size crystallites and the well-ordered fct phase of CoPt alloy. © 1999 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 83 (1998), S. 6611-6613 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Nanostructured NdFeB films were prepared by magnetron sputtering followed by rapid thermal annealing at a ramp rate of 200 °C/s. Isotropically oriented Nd2Fe14B crystallites were formed in the films and coercivities up to 20 kOe and remanence ratios up to 0.8 were obtained. Transmission electron microscopy analysis shows that the majority phase of the magnetic layer in the high coercivity films consists of Nd2Fe14B nanocrystallites with an average size of about 50 nm. These nanocrystallites are believed to be single-domain particles, which are responsible for the high coercivities. MFM measurements show that the domain size is about 500 nm. It is thus indicated that the 50 nm Nd2Fe14B nanocrystallites are strongly exchange-coupled into the 500 nm domains and the high remanence ratio originates from this exchange coupling. © 1998 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 7
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: CoSm films with a Cr underlayer (CoSm//Cr) are promising as future high density recording media.1 It was pointed out that the grain size in media affects the media noise and thermal stability significantly. However, if small grains are exchange coupled to form larger "magnetic grains," the size of these magnetic clusters will be important in noise considerations. Our previous works23 indicated that for CoSm film with Cr underlayer the magnetic grain size is much larger than the 50 Å nanocrystallites and is about the same size as the Cr grain of ∼240 Å in dimension. In the present work, we report our systematic studies of magnetic switching volume and its correlation with magnetic and nanostructural properties for CoSm films. Switching volumes V* were measured with the "field sweep-rate dependence of coercivity Hc," interactions among the magnetic grains were estimated with the so-called ΔM method, and the nanostructures were investigated with atomic force microscopy and transmission electron microscopy. The thickness of CoSm layers, which were sputtered in an Ar pressure PAr=25 mT, is 300 Å for all samples. It is found that as the Cr underlayer thickness dCr increases from 0 Å (without a Cr underlayer) to 200 Å, the V* and ΔMmax decrease (Hc increases) rapidly, i.e., from V* from 9.3×10−18 to 5.7×10−18 cm3, ΔMmax from 1.3 to 0.5 (Hc from 1.4 to 2.3 kOe), respectively, and then gradually as dCr approaches 800 Å. As Ar pressure PAr of the deposition of the Cr underlayer varies from 5 to 30 mT, the V* and ΔMmax have their minima (anisotropy Ku has its maximum) at PAr(similar, equals)9.5 mT. V* shows minima at dCr and PAr values where Hc and Ku have their maxima and ΔMmax has a small value. This behavior can be interpreted with a thermal activation model including interactions between magnetic grains. The relationship between crystallite grain size, magnetic grain V*, and media noise will be discussed. ©1997 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 68 (1996), S. 1153-1155 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Thin films with mostly (Hg,Tl)1Ba2Ca3Cu2O8+δ [(Hg,Tl)-1223] phase have been fabricated by radio frequency magnetron sputtering of precursor films and post-annealing method. The doping of a small amount of thallium in the film is helpful to the formation of the three-layer CuO2 compound. These films have a highly oriented structure with the c-axis perpendicular to the film surface. Resistivity measurements show that the films after annealing at 300 °C for 1 h in O2 have the superconducting transition temperature of Tc(onset)=133 K and Tc(zero)=127 K. Scanning electron micrographs of the film reveal platelike micrometer-size grains coalesce to cover the substrate surface. © 1996 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 70 (1997), S. 135-137 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We have used superparamagnetic magnetic force microscopy (MFM) tips to obtain high spatial resolution MFM images of recording heads. Profiles of the magnetic field gradient above a thin-film recording head under 3 mA bias current to the head and various tip-head distance conditions are presented. At a low tip-head distance, the gap width, gap location, and gap-field structure can be well resolved in these MFM images. Superparamagnetic tips show promise for the magnetic imaging of recording heads with gap widths below 200 nm. © 1997 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 69 (1996), S. 2752-2754 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A process combining hydrofluoric acid (HF) and Ar+ ion milling has been used to make YBa2Cu3Ox/SrTiO3/YBa2Cu3Ox(YBCO/STO/YBCO) multilayer test circuits. Low-angle steps can be readily etched in STO and YBCO films with this process. YBCO lines crossing 5° steps have about the same critical temperature Tc (89–90 K) and critical current density Jc ((approximately-greater-than)1×106 A/cm2 at 86 K) as lines on planar surfaces. Via connections have the same Tc as other circuit components and adequate critical currents for most circuit designs. © 1996 American Institute of Physics.
    Type of Medium: Electronic Resource
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