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  • 1990-1994  (4)
Material
Years
Year
  • 1
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 168 (1993), S. 497-502 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract A radiochemical separation method using Dowex 1×8 (200–400 mesh) has been applied to two tantalum metals of 99.9% purity. While tantalum was still retained on the resin, the elements Na, K, Cr, Mn, Fe, Co and Zn were separated with 2M HF and subsequently the elements Sc, As, Zr, Mo, Eu, W and Hf with a mixture of 0.5M HF and 3M HCl. The separation yields for all impurities was 98–100%. Elemental contents were calculated by a single comparator method using two monitors.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 179 (1994), S. 81-86 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract A radiochemical separation method using an anion exchange resin has been applied to 3N grade Nb for determining nine impurity elements. Five elements (Cr, Fe, Co, Zn and Se) were separated in 2M HF, three elements (Mo, W and Hf) in 32M HF, Nb in 0.5M HF/3M HCl, and Ta in 1M NH4F/4M NH4CCl. The contents of the elements were calculated by a single comparator method using two monitors of Au and Co. The main impurity was revealed to be Ta with a content of over 160 ppm.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 168 (1993), S. 153-161 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract Interferences by uranium fission for95Zr,99Mo,103Ru,140La,141Ce and147Nd have been studied using a single comparator method with two monitors. The effect of the neutron energy spectrum on the interference factor was examined by using the effective activation cross section. All the activities of140La produced during neutron irradiation of uranium were included in the calculation of the factor for lanthanum. The calculated and experimental interference factors are in good agreement within 10% deviation. The results have been applied for the analysis of several rock samples containing uranium in a wide concentration range.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 151 (1991), S. 373-378 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract Instrumental neutron activation analysis has been applied to semiconductor grade silicon to study the concentration levels of impurity elements, the contamination during the single crystal growing process, and the vertical and radial distributions of impurities, along with the decontamination effect in the analysis. Twenty elements of Au, Br, As, W, Cr, Co, Na, Eu, La, Se, Zn, U, Th, Hf, Fe, Sb, Ag, Ce, Tb and Ta have been analyzed in p- and n-type wafers, single crystals and a polycrystal by a single comparator method using two comparators of gold and cobalt. Considerable surface contamination has been found and could be removed by etching the surface with nitric and hydrofluoric acid before and after irradiation. The impurity concentration has been found to be generally increased in the process of single crystal growth. The vertical and radial distributions of impurities have revealed that some impurity elements were more concentrated in the top region of a single crystal rod than in the middle region, and that Br, Cr, La, Eu and Sb were enriched in the central region and As, U and Fe in the outer region.
    Type of Medium: Electronic Resource
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