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Digitale Medien

Non-aqueous, reversed-phase, high-performance, thin-layer chromatography and column liquid chromatography of metal complexes of porphine (1986)

Wakui, Y. ; Saitoh, K. ; Suzuki, N.

Springer

Chromatographia 22 (1986), S. 160-164

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ISSN: 1612-1112

Schlagwort(e): Thin layer chromatography ; Column liquid chromatography ; 21H, 23H-Porphine ; Metalloporphyrin complexes

Quelle: Springer Online Journal Archives 1860-2000

Thema: Chemie und Pharmazie

Notizen: Summary The chromatographic mobility of 21H, 23H-porphine and its Ni(II), Cu(II), Zn(II) and Pd(II) complexes were investigated by high-performance thin-layer chromatography on an octadecyl-bonded, silica gel plate with various polar organic solvents including alcohols, acetonitrile, dimethylsulfoxide and propylenecarbonate. The mobility generally decreases according to the central metal ion of the complex as follows: Zn(II)〉(free porphine)〉Ni(II)〉Pd(II)〉Cu(II). Methanol is a good choice of solvent for the separation of these metal porphine complexes. Successful separation of porphine and the four metal complexes is accomplished within 13 min on a LiChrosorb RP-18 column with methanol eluent.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1007/BF02257319

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