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  • 1980-1984  (7)
  • 1
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract USGS BCR-1 and G-2, NBS 1633a Coal Fly-Ash and a 7-element synthetic standard for biological material have been analysed in this work by reactor NAA, using the k0-standardization method. The analyses were performed independently in the analytical laboratories of the Institute for Nuclear Sciences (INW), Gent, and the Central Research Institute for Physics (KFKI), Budapest. This procedure allowed not only a comparison with the specified data or with other published values, but enabled a check of the consistency of our own results obtained in largely different experimental circumstances. As concluded the k0-standardization method combines general versatility (with respect to irradiation and counting conditions) with good accuracy, while keeping the experimental work as simple as possible. Since the k0 method is a computer-oriented technique, a FORTRAN IV program was designed and applied on a VAX 11/780 machine.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 81 (1984), S. 397-415 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract The present paper deals with the experimental determination and the critical evaluation of Qo, the ratio of the resonance integral (Io) to the 2200 m.s−1 cross-section (σo) for 57 analytically interesting (n, γ) reactions, including a revision and updating of formerly published results for 13 isotopes. Full account is given for deviations from the ideal epithermal neutron flux distribution. The Budapest-Gent cooperative determinations, yielding parallel but independent results, lead to recommended Qo-values with an average uncertainty as low as ∼3%. Finally, with the aid of independently evaluated or measured σo-data, a list of recommended Io-values is given.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 82 (1984), S. 379-383 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract The concept of the effective resonance energy $$\bar E_r $$ , formerly introduced as a parameter in the absolute (e.g. k0-) standardization methodology of (n, γ) activation analysis, is elucidated with respect to dimensioning, accuracy and usefulness.
    Type of Medium: Electronic Resource
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  • 4
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract Isotopic abundance values for50Cr,58Fe and109Ag and the absolute gamma-intensities for51Cr,59Fe and110mAg were evaluated. These evaluated data, together with experimental k0-determinations (i.e. from the “activation method”), made it possible to calculate the following 2200 m.s−1 cross-sections, which considerably deviate from the hitherto generally published ones [between brackets]: $$\begin{gathered} {}^{5 0}Cr(n,\gamma )^{5 1} Cr; \sigma _0 = (15.2 \pm 0.2) barn [cf.:15.8 - 16.0] \hfill \\ {}^{5 8}Fe(n,\gamma )^{5 9} Fe; \sigma _0 = (1.31 \pm 0.03) barn [cf.:1.14 - 1.16] \hfill \\ {}^{1 0 9}Ag(n,\gamma )^{1 1 0 m} Ag;\sigma _0 = (3.89 \pm 0.05) barn [cf.:4.4 - 5.0] \hfill \\ \end{gathered} $$
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 82 (1984), S. 169-179 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract When making use of some single comparator or absolute standardization methods in reactor neutron and in epicadmium neutron activation analysis, the knowledge of the effective resonance energy ( $$\bar E_r $$ ) is essential to correct for the effect of the nonideal epithermal flux distribution on the analysis result. $$\bar E_r $$ can be calculated from neutron resonance data, but when these are incomplete, not accurate or even not known at all, experimental determination should be considered. Such a method, providing both $$\bar E_r $$ and the resonance integral to 2200 ms−1 cross-section ratio (QO), is described in this paper. Results are given for 11 isotopes.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Springer
    Journal of radioanalytical and nuclear chemistry 82 (1984), S. 385-452 
    ISSN: 1588-2780
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Notes: Abstract Recommended k0-factors and related nuclear data for use in (n, γ) activation analysis are given for 72 isotopes. In addition the basic nuclear constants and experimental parameters needed in the k0 standardization method are reviewed. For convenient data reduction, computer programs were developed.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 9 (1980), S. 206-211 
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Multielement thin film standards are made by mixing a solution of different elements and a radioactive tracer (24Na) with the water soluble polymer mehtylcellulose. A film is produced by spreading the liquid mixture evenly on glass plates and letting it dry. Standards of the desired size and shape are punched out. The concentrations of the elements are calculated from the tracer activity. Ten sets of standards containing the elements Na, Mg, Al, Si, P, S, Cl, K, Cs, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Br, Rb, Sr, Ag, Cd, Sn, Sb, Ba and Pb in different groupings have been prepared. Homogeneity and accuracy oof the standards are extensively discussed. The accuracy is also estimated by the alalysis of the standards using several techniques. The precision of the analysis factors derived from the standards is better than 1-2%, while the accuracy for the elements Al, Cl, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Se, Br, Sb, Ba and Pb is found to be better than 5%.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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