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Synthesis of (±) Methyl Fluoromalate (1954)

TAYLOR, N. F. ; KENT, P. W.

[s.l.] : Nature Publishing Group

Nature 174 (1954), S. 401-401

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ISSN: 1476-4687

Source: Nature Archives 1869 - 2009

Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics

Notes: [Auszug] Ethyl ethoxalylfluoroacetate, prepared according to Rivett's method2, was reduced with potassium borohydride (two equivalents) in absolute methanol with vigorous stirring. The temperature of the reaction mixture rose to 50 during the reaction, which was complete after 90 min. Excess dry methanolic ...

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1038/174401a0

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