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Benzotris[1,2,5]thiadiazol in einer Eintopfreaktion aus Benzolhexamin (1990)

Praefcke, Klaus ; Kohne, Bernd ; Korinth, Frank

Weinheim : Wiley-Blackwell

Liebigs Annalen 1990 (1990), S. 203-204

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ISSN: 0170-2041

Keywords: Benzenehexamine ; Benzoselenathiazole ; Benzothiadiazole ; Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Benzotris[1,2,5]thiadiazole in a One-Pot Reaction from BenzenehexamineCondensation of benzenehexamine (1) with thionyl chloride in the presence of pyridine gave the title compound 2 (69% yield) in a one-pot reaction. A similar reaction of 1 with seleninyl chloride or an alternative condensation of 1 with selenium dioxide led to the analogous selenium heterocycle 3 in traces only.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jlac.199019900134

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