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Digitale Medien

NMR studies of the luteinizing hormone-releasing hormone (LH-RH) decapeptide in DMSO solution (1994)

Calzolai, Luigi ; Gaggelli, Elena ; Valensin, Gianni ; [weitere]

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 32 (1994), S. 540-546

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Details

ISSN: 0749-1581

Schlagwort(e): LH-RH ; 1H NMR ; 13C NMR ; Conformational parameters ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: The structure of LH-RH in DMSO solution was studied using 2D NMR experiments at 600 MHz. The 13C NMR spectrum was completely assigned by the combined use of 1H-detected heteronuclear multiple-quantum coherence and 1H-detected multiple-bond heteronuclear multiple-quantum coherence. Measured 1J(CH) values were used to obtain the possible sets of Φ and Ψ dihedral angles. These features, together with some relevant dipolar interactions observed in the ROESY spectrum, were interpreted to provide evidence of some degree of intramolecular structuring.

Zusätzliches Material: 5 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/mrc.1260320908

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