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Digitale Medien

A new 2D NMR method for measurement of JHH coupling constants (1994)

Sørensen, Morten Dahl ; Led, Jens J. ; Sørensen, Ole Winneche

Springer

Journal of biomolecular NMR 4 (1994), S. 135-141

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Details

ISSN: 1573-5001

Schlagwort(e): XLOC ; E.COSY ; 2D NMR ; J coupling constant ; Selective pulse

Quelle: Springer Online Journal Archives 1860-2000

Thema: Biologie , Chemie und Pharmazie

Notizen: Summary A new 2D NMR pulse sequence for E.COSY-type measurement of JHH coupling constants is introduced. It exploits a heteronuclear spin, e.g., 13C, for displacement in the ω1 frequency dimension via a large heteronuclear J coupling. The experiment is demonstrated by application to a heptapeptide at the natural abundance 13C level. It is suitable, for example, for measurement of 3JHH and 4JHH coupling constants in peptides and proteins.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1007/BF00178342

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