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Digitale Medien

NMR 1H relaxation and NOESY studies of spiperone conformational features in solution (1993)

Keller, Charles E. ; Carper, W. Robert

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 31 (1993), S. 566-572

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Details

ISSN: 0749-1581

Schlagwort(e): 1H NMR ; 13C NMR ; 19F NMR ; NOESY ; 2D NMR ; NMR assignments ; Spiperone conformation in solution ; Proton relaxation ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: The high-field 1H, 19F and 13C NMR spectra of spiperone in CDCl3 solution were analyzed with the aid of homonuclear (H-H-COSY) and heteronuclear (H,C-COSY) chemical shift correlation experiments. Multiple through-space intersections were identified using phase-sensitive nuclear Overhauser and exchange spectroscopy (NOESY). Proton relaxation rates and activation energies were determined over the temperature range -60 to 50°C. The chemical shift, NOESY and proton relaxation rate results support the formation of cyclic dimers and multiple spiperone conformations in solution.

Zusätzliches Material: 6 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/mrc.1260310609

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