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  • 1
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 66 (1995), S. 1715-1717 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: The materials science beamline (BL2) at the European Synchrotron Radiation Facility (ESRF) can provide monochromatic or white radiation in the energy range from 7 to 100 keV. The source is a multipole wiggler with a maximum critical energy of 29 keV, producing a radiant power of up to 5 kW. The main optical elements are an adaptive mirror, a monochromator with a liquid nitrogen cooled first crystal followed by a sagittally bent second crystal, and a second mirror including a bender for vertical focusing. The general layout as well as the performance of the beamline optics during the commissioning phase of the ESRF are presented. © 1995 American Institute of Physics.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 66 (1995), S. 2048-2052 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A first adaptive x-ray mirror prototype was built in 1992 and is now installed on the ESRF beamline 2 (Materials Science). This system consists of a water-cooled 1 m long Pt-coated Si mirror, supported by two rows of 11 piezoelectric actuators. The shape of the mirror is continuously monitored by an optical analyzer; its readout being used by a feedback loop in a real-time algorithm. A workstation associated to real-time electronics calculates the relevant parameters for driving the actuators as a function of both the desired shape and the possible thermal deformation due to the incident beam. Preliminary experiments carried out on the wiggler beamline showed that the system runs correctly: the feedback loop permits a control of the mirror shape in the microrad range at a frequency of 10 Hz. Various shapes (cylinder, parabola, or ellipse) can be produced at will to within the above accuracy. The different components of the device are described and the alignment and calibration procedures are discussed. The first results dealing with the properties of the reflected beam (size, divergence, and shape) versus both the calibration quality and the incoming power are presented. © 1995 American Institute of Physics.
    Materialart: Digitale Medien
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  • 3
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 65 (1994), S. 3229-3232 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A new beamline for radiometric applications (e.g., detector calibration and reflectometry) has been installed and characterized at the laboratory of the Physikalisch-Technische Bundesanstalt at the electron storage ring BESSY. The beamline is equipped with a SX700 type plane grating monochromator and a toroidal mirror behind the exit slit of the monochromator for collimating the radiation to allow angle resolved reflectometry. A divergence of 0.1 mrad has been achieved. The beamline has been optimized for high spectral purity of the radiation. Within the photon energy range from 40 to about 1500 eV the total amount of stray light and higher order radiation stays below 1%. A photon flux of up to 1011 s−1 has been measured in the focal point of the toroidal mirror. It corresponds to a radiant power of a few μW and thus allows use of a cryogenic radiometer for detector calibration. The details of the beamline layout and the results of the performance characterization are presented.
    Materialart: Digitale Medien
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  • 4
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 66 (1995), S. 2248-2250 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: At the radiometry laboratory of the Physikalisch-Technische Bundesanstalt (PTB) a reflectometer for the soft x-ray spectral region has been operated for several years utilizing monochromatic radiation of a toroidal grating monochromator or a high-resolution plane grating monochromator. The monochromators cover the photon energy region from 35 to 1500 eV. New challenges due to the development of soft x-ray optical components led to the design of a second reflectometer with advanced capabilities. Samples with a diameter of up to 250 mm can be accommodated. The time required for sample exchange is reduced by using a lock chamber. The feasibility of sample positioning with high precision has been improved. Typical uncertainties of about 1%–2%, e.g., for the reflectance of multilayer mirrors, can be achieved. A detailed description of the reflectometer as well as some typical results showing the performance are presented. © 1995 American Institute of Physics.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 5
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 66 (1995), S. 2147-2150 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: Mechanically ruled or ion-etched blazed diffraction gratings can be coated with multilayer reflectors to increase their on-blaze efficiency in the soft x-ray and extreme ultraviolet (EUV) spectral regions. The quality of the groove facets produced by these conventional manufacturing techniques precludes their use in high spectral orders to achieve high resolving power, i.e., as echelles. However, coarse gratings fabricated in crystalline silicon by orientation-dependent etching have excellent groove profile and extremely smooth facets, which make them ideal for coating with multilayers for use as echelles at short wavelengths. Such a grating was coated with tungsten-carbon multilayers for use at soft x-ray wavelengths near the carbon K edge. It was evaluated using both a reflectometer based on a laser-produced plasma source and with synchrotron radiation. In the 50–220 A(ring) wavelength region, diffraction orders up to the 61st were observed, allowing the grating performance to be compared with theoretical predictions. Such multilayer-coated echelles offer the possibility of extremely high spectral resolving power in the EUV and soft x-ray region. © 1995 American Institute of Physics.
    Materialart: Digitale Medien
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  • 6
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 66 (1995), S. 4736-4737 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: For the first time, the spectral responsivity of the same silicon n on p photodiode has been determined with self-calibration techniques in the visible and soft x-ray regions. Together with results from other calibrations the spectral responsivity is presented for the whole photon energy range from 1.2 eV to 3 keV. © 1995 American Institute of Physics.
    Materialart: Digitale Medien
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  • 7
    ISSN: 1089-7550
    Quelle: AIP Digital Archive
    Thema: Physik
    Notizen: We report the results of structural, chemical, and extreme ultraviolet (EUV) characterization of Si/Mo multilayers grown by sputtering and by UHV evaporation. This study includes mirrors designed for normal incidence with peak reflectivities Rpeak between 22 and 24 nm, and 45° mirrors having Rpeak between 16 and 19 nm. The deposition conditions were varied to produce multilayers with a wide range of interface morphologies. A variety of techniques were used to determine the structure and composition of the multilayers, including x-ray diffraction, transmission electron microscopy, Rutherford backscattering spectroscopy, and Auger depth profiling. All of the mirrors have amorphous Si layers and polycrystalline Mo layers with thin amorphous alloy interlayers. We obtain good fits to the low-angle x-ray diffraction data only when these interlayers are taken into account. The best sputter-deposited mirrors were made at the lowest Ar pressure studied, 3 mTorr. The best evaporated mirrors were produced at a substrate temperature of 200 °C. The EUV reflectivity as a function of wavelength was measured using synchrotron radiation. Both the multilayer structure and surface contamination significantly affect the EUV reflectivity, and must be considered to obtain good fits to the reflectivity curves. The best 45° mirror had a peak reflectivity of 53% at 18.6 nm for 100% S-polarized light, and the best normal-incidence mirror had a peak reflectivity of 33% at 23.6 nm.
    Materialart: Digitale Medien
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  • 8
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 63 (1992), S. 797-801 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A self-calibration procedure is presented for semiconductor photodiodes to be used as detectors in the soft x-ray region. In this procedure the spectral responsivity is calculated according to a model from experimentally accessible parameters of the detector. The thicknesses of the dead layer and the space charge region as well as the diffusion length have been determined in monochromatic radiation by investigating the angular dependence of the photocurrent. The mean energy for electron-hole pair creation has been determined in calculable undispersed synchrotron radiation of the primary standard source BESSY. The obtained uncertainties of the spectral responsivity in the photon energy region between 150 and 2500 eV are ≤4.2% for newly developed Si n on p diodes and ≤6% for GaAsP/Au diodes. The calibrated photodiodes were used to determine the quantum efficiency of photoemissive gold diodes which is up to four orders of magnitude lower than that of semiconductor photodiodes.
    Materialart: Digitale Medien
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  • 9
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 60 (1989), S. 2287-2290 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: The response function of a Si(Li) detector has been measured in the photon energy range 0.9–5 keV using monochromatized synchrotron radiation at a double crystal monochromator. The response is described by a hypermet function and the spectral dependence of its parameters is presented. The quantum detection efficiency of the detector is determined from measurements in the undispersed synchrotron radiation of the electron storage ring BESSY, which is a primary radiometric standard.
    Materialart: Digitale Medien
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  • 10
    Digitale Medien
    Digitale Medien
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 60 (1989), S. 2291-2294 
    ISSN: 1089-7623
    Quelle: AIP Digital Archive
    Thema: Physik , Elektrotechnik, Elektronik, Nachrichtentechnik
    Notizen: A new procedure for the calibration of photon detectors is presented, based on the electron storage ring BESSY as a calculable radiometric standard source and an energy dispersive Si(Li) detector. The quantum detection efficiency of the Si(Li) detector is determined in the undispersed synchrotron radiation of BESSY, and the detector to be calibrated is compared to the Si(Li) detector in monochromatic radiation. The procedure is applied in the photon energy range from 800 to 3500 eV to calibrate semiconductor photodiodes which are promising as transfer standard detectors due to their high quantum efficiency, excellent stability in intense radiation, and insensitiveness to surface contaminations.
    Materialart: Digitale Medien
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