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NMR study of the monomer - dimer equilibria of dimethylnitrosobenzenes in solution. Identification of mixed azodioxy dimeric species (1989)

Orrell, Keith G. ; Stephenson, David ; Rault, Thierry

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 27 (1989), S. 368-376

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ISSN: 0749-1581

Schlagwort(e): 1H NMR ; 13C NMR ; 2,6-Dimethylnitrosobenzene ; 3,5-Dimethylnitrosobenzene ; Monomer-dimer equilibria ; Mixed azodioxy dimers ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: The monomer-dimer equilibria of 2,6- and 3,5-dimethylnitrosobenzenes in CDCI3 solution were investigated by 1H and/or 13C NMR spectroscopy. The mixed systems nitrosobenzene + 2,6-dimethylnitrosobenzene and 2,6-dimethylnitrosobenzene + 3,5-dimethylnitrosobenzene were also studied, and mixed azodioxy dimers were identified. In all systems exchange occurs exclusively between dimer and monomer species, rates and activation energies being calculated from time-dependent 1H 1D spectra and/or 1H 2D-EXSY spectra measured at different temperatures.

Zusätzliches Material: 6 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/mrc.1260270413

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