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Digitale Medien

Structural effects on ESR hyperfine coupling constants of some dithiazolidinyl free radicals (1989)

Krebber, Angelika M. L. ; Sutcliffe, Leslie H. ; Lubitz, Wolfgang ; [weitere]

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 27 (1989), S. 288-294

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Details

ISSN: 0749-1581

Schlagwort(e): ESR ; ENDOR/TRIPLE ; Dithiazolidinyl free radicals ; Sulphur-nitrogen heterocycles ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: A series of related dithiazolidin-2-yl free radicals prepared from cyclic strained alkenes and tetrasulphur dinitride, and an attempt was made to relate the nitrogen and proton hyperfine coupling constants to the radical structures. The radical made from dimethoxybenzonorbornadiene was studied by ENDOR and it was found that isotopic substitution with 15N gives well resolved ENDOR spectra; the TRIPLE measurements showed that the 14N coupling constants are positive whereas all the resolved proton coupling constants are negative.

Zusätzliches Material: 4 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/mrc.1260270318

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