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Synthesis of the Glycopeptide Partial Sequence A80-A84 of Human Fibroblast Interferon (1985)

Kunz, Horst ; Waldmann, Herbert

New York, NY : Wiley-Blackwell

Helvetica Chimica Acta 68 (1985), S. 618-622

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ISSN: 0018-019X

Keywords: Chemistry ; Organic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The glycopentapeptide H-(GlcNAcβ1-)Asn-Glu-Thr-Ile-Val-OH (10) representing the partial sequence A80-A84 of human fibroblast interferon was synthesized using the newly developed allyl-ester protection of carboxy functions. The allyl esters, which are stable to acids and to bases, can be cleaved under very mild, neutral conditions using tris(triphenylphosphine)rhodium(I) chloride or tetrakis(triphenylphosphine)palladium(0) as a catalyst. This synthetic method opens up a preparative route to glycopeptide model structures of glycoproteins of high biological interest.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/hlca.19850680314

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