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Digitale Medien

Preparative HPLC. Part 1: A comparison of three types of equipment for the purification of steroids (1984)

Matlin, S. A. ; Chan, L.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 7 (1984), S. 570-576

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Details

ISSN: 0935-6304

Schlagwort(e): Preparative high performance liquid chromatography, HPLC ; Steroid esters ; Long-acting contraceptives ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: Two commercial preparative liquid chromatographs have been evaluated for gram-scale purification of steroid esters. The Jobin-Yvon and Waters chromatographs both allow fast separations. Neither system has a high intrinsic column efficiency, but the resolving power of the Waters system can be increased by the use of recycle. A laboratory-assembled preparative liquid chromatograph is described which is economical both in construction and operation, versatile, and considerably more efficient than the two commercial alternatives for single runs on up to a gram scale.

Zusätzliches Material: 6 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/jhrc.1240071005

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