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Novel Nitrido- and Oxo(phthalocyaninato) Complexes of Molybdenum, Tungsten and Rhenium (2000)

Frick, Karsten ; Verma, Sanjiv ; Sundermeyer, Jörg ; [et al.]

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 2000 (2000), S. 1025-1030

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Details

ISSN: 1434-1948

Keywords: Phthalocyanines ; Nitrides ; Oxo complexes ; Rhenium ; Molybdenum ; Tungsten ; Chemistry ; General Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The synthesis of new nitrido(phthalocyaninato)molybdenum (1-4) and -tungsten complexes (5-7) starting from the corresponding phthalonitriles and MNCl3 (M = Mo, W) is reported. In addition, the reaction of (tBu4Pc)WN (6) with PPh3 leading, after several steps, to the diamagnetic compound (tBu4Pc)WO (7) is described. The reaction of (tBu4Pc)ReN (9) with PPh3 leads to [(tBu4Pc)ReO]2 (12), and of [(C5H11)8Pc]ReN (10) with PPh3 leads, under different conditions, to {[(C5H11)8Pc]ReO}2O (11).

Additional Material: 3 Ill.

Type of Medium: Electronic Resource

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