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Borohydride reduction of alkyl phenyl ketones within a reversed-phase liquid chomatographic column (1990)

Jaeger, David A. ; Clennan, Malgorzata Wegrzyn

Chichester : Wiley-Blackwell

Journal of Physical Organic Chemistry 3 (1990), S. 594-598

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ISSN: 0894-3230

Keywords: Organic Chemistry ; Physical Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology , Physics

Notes: The reductions of propiophenone and octanophenone to 1-phenylpropan-1-ol and 1-phenyloctan-1-ol, respectively, with sodium borohydride and tetrabutylammonium borohydride were performed on a reverse-phase highperformance liquid chromatographic (HPLC) column of macroporous 10-μm poly(styrene-divinylbenzene) undr HLPC conditions. In these reactions a lower concentration of tetrabutylammonium borohydride than of sodium borohydride was needed to effect the same extent of reduction, and modest substrate selectivity was obtained.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/poc.610030907

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