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Dimeric oxotrifluoromolybdate: The crystal structure of [MoO(S2CNEt2)3]2Mo2O4F6 (1975)

Dirand, Jocelyne ; Ricard, Louis ; Weiss, Raymond

Springer

Transition metal chemistry 1 (1975), S. 2-5

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ISSN: 1572-901X

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Summary The spontaneous decomposition of the compounds MoOF2(S2CNR2)2, where R = Et or n-Pr yields salts containing the new cation [MoO(S2CNR2)3]+ and the dimeric anion [Mo2O4F6]2− The structure of the ethyl derivative has been determined by x-ray diffraction techniques. It crystallizes in space group C2/c with a = 27.3 56(4) Å, b = 17.292(3) Å, c = 12.716(3) A,β = 103.76(3)°. All atoms, including the thirty hydrogen atoms, were used in a least-squares procedure with convergence to a conventional R factor of 0.045. The i.r. and far i.r. spectra are discussed.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01753071

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