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Disordered crystal structure of chlorodifluoroacetamide (1976)

Kalyanaraman, B. ; Kispert, L. D. ; Atwood, J. L.

Springer

Journal of chemical crystallography 6 (1976), S. 311-316

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The crystal structure of chlorodifluoroacetamide has been determined from three-dimensional counter data, and refined by full-matrix least-squares techniques. The crystals belong to the monoclinic space groupP21/n witha = 7.401(6),b = 8.123(6),c = 8.431(6) Å, β = 104.48(5) °, andD = 1.52 gcm−3 forZ = 4. The finalR factor for 650 observed reflections is 0.059. The compound exists with a rotational disorder in the -CClF2 group about the C-C bond. The occupancy factors for the major and minor conformations are 0.74 and 0.24, respectively.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01292368

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