ISSN:
1612-1112
Schlagwort(e):
Column liquid chromatography
;
Ion exchange chromatography
;
Anion-exchange chromatography
;
Arsenic compounds
;
Flame atomic absorption detector
Quelle:
Springer Online Journal Archives 1860-2000
Thema:
Chemie und Pharmazie
Notizen:
Summary Identification and quantification of arsenic compunds was performed with high- performance liquid chromatography (HPLC) and flame atomic absorption spectrometry (FAAS) as element-specific detector. Arsenous acid, methylarsonic acid, dimethylarsinic acid, arsenic acid, arsenobetaine, and arsenocholine were separated on two anion-exchange columns (Synchropak Q 300 and PRP-X 100) with different binary organic acids as mobile phases. The infleunce of chromatographic parameters, such as pH and the concentration of the mobile phase were investigated. An unusual chromatographic behavior of arsenous acid was observed when tartaric acid was used as mobile phase.
Materialart:
Digitale Medien
URL:
http://dx.doi.org/10.1007/BF02466529