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  • Articles: DFG German National Licenses  (28)
  • Chemistry  (24)
  • millimeter-wave  (4)
  • 1
    Electronic Resource
    Electronic Resource
    Continuously tunable, split-cavity gyrotrons (1985)
    Springer
    International journal of infrared and millimeter waves 6 (1985), S. 1237-1254 
    Details
    ISSN: 1572-9559
    Keywords: gyrotron ; millimeter-wave ; microwave ; electron cyclotron resonance maser ; resonant cavities ; frequency tuning
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract The cavity of the University of Sydney gyrotron, GYROTRON IIIB, is split in two longitudinally to allow and frequency that lies between the fixed cavity resonances to be accessed by mechanically changing the separation of the two halves. The rate of change in resonant frequency with separation is greatest if the minor axis of the cavity cross-section is the one undergoing change. Results obtained with the latest cavity demonstrate this and show excellent agreement with theory.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01013212
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    Tuneable millimeter-wave gyrotrons (1982)
    Springer
    International journal of infrared and millimeter waves 3 (1982), S. 725-734 
    Details
    ISSN: 1572-9559
    Keywords: gyrotron ; millimeter-wave ; microwave cavities ; microwaves ; electron cyclotron maser
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract In the course of developing a low-power, tuneable millimeter-wave source, two gyrotrons have been constructed. Gyrotron I was a fixed-frequency device operating at 120 GHz while Gyrotron II produced more than 20 lines in the frequency range 130 to 260 GHz. The design of tuneable gyrotrons is discussed with reference to the Gyrotron II results.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01009730
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  • 3
    Electronic Resource
    Electronic Resource
    Frequency detuning measurements in a low-power gyrotron (1983)
    Springer
    International journal of infrared and millimeter waves 4 (1983), S. 891-900 
    Details
    ISSN: 1572-9559
    Keywords: gyrotron ; millimeter-wave ; microwave ; electron cyclotron resonance maser ; frequency detuning ; frequency pulling
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract Frequency detuning in the University of Sydney Gyrotron II has been measured for a number of modes in the vicinity of the TE0 14 1 mode at 183 GHz. The main features of the observations agree with theory and the importance of a detailed knowledge of the electron velocity distribution and the cavity Q's is established.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01009314
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  • 4
    Electronic Resource
    Electronic Resource
    Observation of mode conversion in gyrotrons (1985)
    Springer
    International journal of infrared and millimeter waves 6 (1985), S. 1255-1266 
    Details
    ISSN: 1572-9559
    Keywords: gyrotron ; millimeter-wave ; microwave ; electron cyclotron resonance maser ; mode conversion ; far-field imaging
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract The observed output power levels in the University of Sydney's gyrotron can be accounted for only by including the effects of mode conversion at waveguidetaper transitions in the vicinity of the resonant cavity. A series of measurements taken from liquid-crystal images of the microwave fields beyond the output window confirms this.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01013213
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  • 5
    Electronic Resource
    Electronic Resource
    FAB and tandem mass spectrometry for endorphin- and ACTH peptides of molecular weight to 2000 (1988)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 15 (1988), S. 649-657 
    Details
    ISSN: 0887-6134
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Four β-endorphins (β-endorphin 6-17, 2-17, 1-16, and 1-17) and two adrenocorticotropic hormone (ACTH) peptides (ACTH 1-10 and (1-16)-NH2) were studied by using fast atom bombardment coupled with tandem mass spectrometry. The capability to reproduce metastable ion and collisionally activated decomposition spectra on two different commercial sector mass spectrometers in two different laboratories was found to be acceptable (deviations in relative abundance are less than ± 50%). The endorphin peptides fragment metastably or upon collisional activation to give abundant B-series ions as well as Y-series ions, whereas Y-series ions are the principal ionic species produced upon the desorption by fast atom bombardment. The ACTH peptides also fragment to give Y-series ions, but of relatively low abundance compared to those from the endorphins. For both sets of peptides, high-energy collisionally activated decomposition and metastable ion decomposition daughter ion spectra are precise, structurally informative - even for peptides up to m/z 2000 - and complementary to spectra of daughter ions produced by desorption ionization alone.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200151203
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  • 6
    Electronic Resource
    Electronic Resource
    Fast atom bombardment and tandem mass spectrometry for structure determination: Remote site fragmentation of steroid conjugates and bile salts (1988)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 15 (1988), S. 89-98 
    Details
    ISSN: 0887-6134
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A series of 35 steroid conjugates (sulfates and glucuronides) and bile salts were investigated by using fast atom bombardment and tandem mass spectrometry. Collisional activation of the [M - H]- anions of sulfate conjugates and bile salts predominantly yields fragment ions arising by reactions occurring remote from the charge site. These reactions are sometimes sensitive to differences in stereochemistry at positions remote from the charge site and are useful for positional isomer differentiation. On the other hand, collisional activation of the [M - H]- anions of the glucouronide conjugates leads primarily to charge-driven fragementations.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/bms.1200150206
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  • 7
    Electronic Resource
    Electronic Resource
    Synthese von Hydroxyguanidinen aus Chlorformamidinen und OximenTeil der Dissertation M. Gross, Martin-Luther-Universität, Halle 1971. (1974)
    New York, NY : Wiley-Blackwell
    Journal für Praktische Chemie/Chemiker-Zeitung 316 (1974), S. 434-442 
    Details
    ISSN: 0021-8383
    Keywords: Chemistry ; Organic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: N2-Aryl-N1,N1-dialkylchlorformamidine 1 reagieren mit Oximen über hydrolyseempfindliche Zwischenprodukte zu 2-Hydroxy-1-aryl-3,3-dialkylguanidinen 3.Diese Hydroxyguanidine bilden mit Benzoylchlorid O- und O,N-acylierte Verbindungen, mit Chlorameisensäureestern entstehen 3-Dialkylamino-4-aryl-5-oxo-Δ2-1,2,4-oxadiazoline 7. Die Reaktion mit Alkylhalogeniden führt zu 2-Alkoxy-1-aryl-3,3-dialkylguanidinen 8, und die katalytische Hydrierung liefert 1-Aryl-3,3-dialkylguanidine. Bei der Abspaltung der Oximinogruppe im saure Medium in Gegenwart von Oxydationsmitteln entstehen entsprechend substituierte Harnstoffe.
    Additional Material: 3 Tab.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/prac.19743160311
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  • 8
    Electronic Resource
    Electronic Resource
    Reactions of propene and cyclopropane radical cations with neutral ethylene (1993)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 28 (1993), S. 185-192 
    Details
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The gas-phase reactions of propene and cyclopropane radical cations with neutral ethylene were investigated by using Fourier transform, chemical ionization and tandem mass spectrometries. Both reactions form covalent C5H10 adduct ions. The adduct ions are hypothesized to form initially as distonic radical cations that isomerize via a substituted cyclopropane intermediate and are detected as the most stable C5H10 isomer, the 2-methylbut-2-ene radical cation. The rate constant for each reaction is approximately 20% of the theoretical collision rate, indicating that product ions are formed in one out of every five collisions of the C3H6 radical cations with neutral C2H4.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/oms.1210280309
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  • 9
    Electronic Resource
    Electronic Resource
    Anodic oxidation of mercury in the presence of monocyclic ligands in propylene carbonate (1989)
    Weinheim : Wiley-Blackwell
    Electroanalysis 1 (1989), S. 493-499 
    Details
    ISSN: 1040-0397
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A series of 12 macrocycles containing 4, 6, or 8 N, S, and O heteroatoms (with increasing size from 14 to 24 atoms in the cycle) was studied to ascertain size and heteroatoms effects on the formation and 14 redox characteristics of their mercuric complexes. The concentration dependence of anodic currents at mercury electrodes in solutions of these ligands led to the determination of the formation constants of the complexes generated according to the folling of \documentclass{article}\pagestyle{empty}\begin{document}$$ {\rm Hg} \mathbin{\lower.3ex\hbox{$\buildrel\textstyle\rightarrow\over {\smash{\leftarrow}\vphantom{_{\vbox to.5ex{\vss}}}}$}} {\rm Hg}^{{\rm 2 + }} {\rm + 2e}^{\rm - } {\rm,}\,{\rm Hg}^{{\rm 2 + }} {\rm + jL} \mathbin{\lower.3ex\hbox{$\buildrel\textstyle\rightarrow\over {\smash{\leftarrow}\vphantom{_{\vbox to.5ex{\vss}}}}$}} {\rm (HgL}_{\rm j} {\rm)}^{{\rm 2 + }} $$\end{document} In propylene carbonate, the resulting mercuric complexes were stable (log Ks up to 40) mono- and dinuclear species. Their stability depends both on the nature of the heteroatoms and on the size of the macrocycle. For identical ligand sizes, the stability sequence N 〉 S 〉 O was established for mercuric complexes.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/elan.1140010604
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  • 10
    Electronic Resource
    Electronic Resource
    Elucidation of some fragmentations of small peptides using sequential mass spectrometry on a hybrid instrument (1989)
    New York, NY : Wiley-Blackwell
    Rapid Communications in Mass Spectrometry 3 (1989), S. 217-221 
    Details
    ISSN: 0951-4198
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Sequential daughter-ion-scanning analyses of small peptides have been performed using a hybrid tandem instrument of BEqQ configuration. Precursor ions are selected by B and allowed or induced (by high-energy collisional activation) to decompose in the region preceding E. Decoupling of E from the accelerating voltage permits the selection of the first-generation daughter ion whilst retaining appropriate float voltages for the quadrupole assemblies. The daughter ion selected by E is further subjected to low-energy collisional-activation dissociation (CAD) in q and the fragment-ion spectrum is obtained by scanning Q. The sequential daughter-ion-scanning technique has been used to establish that ‘internal’ fragments of the types, (AY′) and (BY′), are formed via initial Y-type cleavage. Fragmentation of a protonated peptide (angiotensin III) by loss of the C-terminal amino acid residue, yielding a (Bn′ + OH) ion, is reported for the first time. This process is analogous to that previously described for metal-cationized peptides.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/rcm.1290030704
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