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  • 1995-1999  (3)
  • Chemistry  (2)
  • Mitochondrial swelling
  • Purkinje fibres
  • 1
    Electronic Resource
    Electronic Resource
    Effects of ischaemia and preservation on the ultrastructure of the bronchiolar epithelium (1996)
    Springer
    Virchows Archiv 429 (1996), S. 109-118 
    Details
    ISSN: 1432-2307
    Keywords: Lung-transplantation pathology ; Bronchi-epithelium ; Ischaemia ; Mitochondrial swelling ; Scanning electron microscopy ; Transmission electron microscopy
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Abstract In ten cases of clinical human single-lung transplantation, the nontransplanted Euro-Collins-preserved contralateral lungs were examined using electron microscopy to determine the effects of ischaemia on the bronchiolar epithelium. Existing structural damage at the time of transplantation was characterized using this approach, and nine nonpreserved canine single lungs were also investigated to identify the impact of ischaemia. The study revealed a significant correlation between the duration of ischaemia and the mitochondrial surface-to-volume ratio, which can serve as a morphometric criterion for mitochondrial damage, in canine lungs. However, this correlation was not found in the human donor lungs. Further examination of human donor lungs showed slight to moderate damage to the endoplasmic reticulum and nuclear chromatin. In addition, various degrees of damage to mitochondrial structure, ranging from inconspicuous to severe, were found. The mitochondrial surface-to-volume ratio can be considered to be a suitable criterion for the quantification of ischaemic damage of the bronchiolar epithelium under experimental conditions. Ultrastructural analysis of human donor lungs revealed intact bronchiolar epithelial cell structures at the time of transplantation, reflecting adequate organ preservation with Euro-Collins solution.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00192433
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  • 2
    Electronic Resource
    Electronic Resource
    STM-induced Annealing and Nanoextrusion in nm-Period Multilayers (1997)
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 25 (1997), S. 596-605 
    Details
    ISSN: 0142-2421
    Keywords: nanotechnology ; scanning tunnelling microscopy ; thin films ; metal multilayers ; annealing ; extrusion ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Nanometre-period nickel-carbon multilayers were used as a writing medium for nanostructure fabrication induced by gap voltage manipulations in a scanning tunnelling microscope. The choice of immiscible sample materials provided high-stability written metallic structures. Two well-distinguished hillock-like nanostructure types were observed, depending on the tip-sample separation, polarity and interaction time. Relatively slow local annealing under positive sample potential without a direct tip-sample contact resulted in the formation of nanostructures of 〈20 nm wide and a few nanometres high. Rapid melting followed by metal melt extrusion was observed if the tip contacted the sample during the nanostructure formation, independent of the polarity of the applied voltage. These metallic-like structures were tens of nanometres high and had a good electronic contrast to the initial carbon-coated surface. No traces of tip material were found in the processed areas. The shape of the nanostructures and the threshold voltage of their formation were strongly dependent on the tip condition. Possible courses of nanostructure formation are discussed.© 1997 John Wiley & Sons, Ltd.
    Additional Material: 15 Ill.
    Type of Medium: Electronic Resource
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    Paper (German National Licenses)
  • 3
    Electronic Resource
    Electronic Resource
    Die Reaktion von SeCl4 mit Übergangsmetalltetrachloriden. Synthese und Kristallstrukturen von (SeCl3)2MCl6 mit M = Zr, Hf, Mo, ReProfessor Gerhard Thiele zum 60. Geburtstag gewidmet (1996)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 622 (1996), S. 292-296 
    Details
    ISSN: 0044-2313
    Keywords: Trichloroselenium(+) ; Hexachlorozirconate(2-) ; Hexachlorohafnate(2-) ; Hexachloromolybdate(2-) ; Hexachlororhenate(2-) ; Synthesis ; Crystal structure ; magnetic properties ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: The Reaction of SeCl4 with Transition Metal Tetrachlorides. Synthesis and Crystal Structures of (SeCl3)2MCl6 with M = Zr, Hf, Mo, ReThe transition metal tetrachlorides ZrCl4, HfCl4 and MoCl4 react with SeCl4 in closed ampoules at temperatures of 140°C to (SeCl3)2MCl6 (M = Zr, Hf, Mo) which are all isotypic and crystallize in the (SeCl3)2ReCl6 structure type (orthorhombic, Fdd2, Z = 8, lattice constants for M = Zr: a = 1165.7(1)pm, b = 1287.2(2)pm, c = 2180.2(2)pm; for M = Hf: a = 1162.9(2)pm, b = 1285.0(2)pm, c = 2178.2(3)pm; for M = Mo: a = 1153.8(1)pm, b = 1267.7(1)pm, c = 2147.4(2)pm). The Cl- ions form a hexagonal closest packing with one fourth of the octahedral holes filled by Se4+ and M4+ in an ordered way. The MCl6 octahedra are regular, the SeCl6 octahedra are distorted with 3 short and 3 long Se—Cl bonds (mean 215 pm and 287 pm). The structures can thus be regarded as built of SeCl3+ and MCl62- ions. Magnetic susceptibility measurements show for M = Zr the expected diamagnetic behavior, for M = Mo and Re paramagnetic behavior according to the Curie-Weiss law with magnetic moments of 2.5 B. M. for M = Mo and 3.7 B. M. for M = Re corresponding to 2 and 3 unpaired electrons respectivly.
    Notes: Die Übergangsmetalltetrachloride ZrCl4, HfCl4 und MoCl4 reagieren mit SeCl4 in geschlossenen Ampullen bei Temperaturen von 140°C zu (SeCl3)2MCl6 (M = Zr, Hf, Mo), die alle isotyp sind und im (SeCl3)2ReCl6-Typ kristallisieren (orthorhombisch, Fdd2, Z = 8, Gitterkonstanten für M = Zr: a = 1165,7(1)pm, b = 1287,2(2)pm, c = 2180,2(2)pm; für M = Hf: a = 1162,9(2)pm, b = 1285,0(2)pm, c = 2178,2(3)pm; für M = Mo: a = 1153,8(1)pm, b = 1267,7(1)pm, c = 2147,4(2)pm). Die Anionen bilden eine hexagonal dichteste Kugelpackung, in der ein Viertel der Oktaederlücken geordnet von Se4+ und M4+ besetzt ist. Die MCl6-Oktaeder sind regelmäßig, die SeCl6-Oktaeder mit drei kurzen und drei langen Se—Cl-Abständen (im Mittel 215 pm und 287 pm) stark verzerrt. Die Strukturen können damit als aus SeCl3+- und MCl62--Ionen aufgebaut betrachtet werden. Die Messung der magnetischen Suszeptibilität ergibt für (SeCl3)2ZrCl6 den erwarteten Diamagnetismus, für (SeCl3)2MoCl6 und (SeCl3)2ReCl6 paramagnetisches Verhalten nach dem Curie-Weiss-Gesetz und magnetischen Momenten von 2,5 B.M. entsprechend 2 ungepaarten Elektronen für M = Mo und 3,7 B. M. entsprechend 3 ungepaarten Elektronen für M = Re.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19966220215
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