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  • 1
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 83 (2000), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Discrete element modeling was used to establish the effects of size distribution on loose packing fraction during the fall of 5000 to 10 000 agglomerates. Monosized distributions exhibited slightly lower packing fraction than “narrow” distributions. However, broad distributions always produced the lowest packing fraction. The application of radius ratio rules had an effect opposite to that intended. Smaller fines had a disproportionately large effect on packing fraction, an effect attributed to gaslike behavior. Gravity-driven random packing in ceramic agglomerates was governed by a combination of “bridge” formation and kinetic agglomerate–agglomerate interactions, not by geometric constraints.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 87 (2004), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Localized densification and compaction efficiency at high pressures was studied using X-ray computed tomography. Stage III begins with the initiation of a region of uniform average density within the overall high-density zone. No further densification occurs in this region; additional pressure is transmitted into adjacent, less-dense zones and the die wall. This localized increase in wall friction continuously decreases compaction efficiency. Discrete element modeling was used to visualize force transfer. The transition was governed by events that ranged from the microscale to the macroscale. Terapascal levels of pressure were required to produce a uniform compact.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 83 (2000), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: This study proves that initial density gradients have lasting detrimental effects on final dimensional tolerances. X-ray computed tomography has been used to quantify changes in density following sintering; associated dimensional changes have been monitored using a laser micrometer. Nonuniformities present in the green state are still present at an overall relative density of ∼73%; in fact, these nonuniformities are exaggerated. Major losses of dimensional tolerance are triggered by the initial density gradients.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 83 (2000), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The present work utilized X-ray computed tomography (CT) and in situ laser dilatometry to correlate internal structural changes with dimensional variation during thermally driven binder removal. Nonuniform agglomerate arrangement and deformation introduced during compaction provide density gradients that drive binder migration. Simultaneously, density undergoes a slight decrease accompanied by a 1.0% loss in dimensional tolerance. This loss and CT difference images show that capillary forces generated during binder melting can change internal density distribution. This change in density has important implications for the binder removal process.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 81 (1998), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: X-ray computed tomography was used to quantify the internal structure of compacts made from poly(vinyl alcohol)-containing spray-dried agglomerates at specific levels of humidity. High humidities increased the average density but decreased the uniformity of the density distribution. Lower levels of humidity generally produced more diffuse high density zones. Internal uniformity is superior at lower humidities where agglomerate fracture is more common than gradual agglomerate deformation. SEM has been used to determine zone-specific agglomerate behavior at 0% and 98% relative humidity. These results can be used to connect gradient development to compaction curve behavior.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 83 (2000), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Tungsten marker layers and X-ray computed tomography were used to monitor the compaction of spray-dried alumina. Local density changes and compaction curves show that the well-known Stage I—II transition indicates an alteration in the direction of transmitted pressure through the uppermost layer. Stage I pressure is dispersed in local agglomerate contacts until “pockets” of low density are eliminated. In Stage II, these deformed/fragmented agglomerates behave as a continuous body and interact with wall friction to transmit pressure nonuniformly into the bulk. Discrete element simulations reproduced the compaction curves and provided clear explanation of the density distribution development.
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 83 (2000), S. 0 
    ISSN: 1551-2916
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: X-ray computed tomography (CT) and mercury porosimetry were combined to connect density gradients and the distribution of open porosity in a sintered compact. CT clearly showed that open porosity follows the initial distribution of low-density zones. Mercury porosimetry detected three distinct levels of porosity. Microstructural examination correlated the porosity level with the coordination of (i) two to three or (ii) multiple grains around pores. This combination of techniques provides a novel tool for the study of pore and density-gradient evolution during sintering.
    Type of Medium: Electronic Resource
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