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  • 1
    Electronic Resource
    Electronic Resource
    s.l. : American Chemical Society
    Environmental science & technology 27 (1993), S. 539-547 
    ISSN: 1520-5851
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 76 (1994), S. 7636-7638 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: In scanning electron microscopy and low voltage point-projection microscopy there is considerable interest in estimating beam damage which can be related to the energy deposited in the specimen. We derive an expression for the energy deposition using the electron transport equation and give results for beam energies of 1–10 kV incident on 100 and 200 nm carbon films. The elastic scattering was modeled using a Rutherford cross section and the inelastic scattering cross section was derived from the Bethe stopping power equation. For the 100-nm-thick amorphous carbon film 90% of the incident beam energy is deposited in the sample at 2 keV, but at 6 keV only 20% of the energy is deposited. The 200 nm sample exhibited a similar curve with 20% deposition occurring at 9 keV. Our calculations show the same variation with beam energy as reported experimental results. © 1994 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : International Union of Crystallography (IUCr)
    Acta crystallographica 55 (1999), S. 160-167 
    ISSN: 1600-5724
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Notes: Charge densities and crystal structures can be determined routinely from X-ray diffraction as X-ray scattering is relatively weak and single scattering can be assumed. The strong dynamical diffraction of high-energy electrons has prevented electron diffraction from being used in the same way. Dynamical diffraction describes both the propagation of the Bragg diffracted wave in the crystal and the scattering by the crystal potential. The balance between these two processes changes as a function of voltage due to relativistic effects. The difference in diffracted intensities recorded at two voltages is shown to be directly proportional to the crystal potential. This is confirmed by calculations using first-order perturbation theory which show negligible differences compared to exact calculation. It should therefore be possible to use differences in intensity measured as a function of voltage to determine the crystal potential directly. If the full complex wave function is available, then there is a particularly simple procedure to recover the potential, even under dynamical conditions.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 13 (1984), S. 33-37 
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The use of peak-to-background ratios has been suggested for the analysis of particles or rough surfaces as the peak-to-background ratio is assumed to be independent of geometry. The validity of this assumption is examined for flat specimens. It is shown that the peak-to-background ratio does not vary much with sample orientation but does vary with voltage, tending to a limit at high voltages. Methods of analysis using the peak-to-background ratio are proposed and the effects of fluorescence are discussed.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    Microscopy Research and Technique 21 (1992), S. 166-170 
    ISSN: 1059-910X
    Keywords: Protein crystals ; Crystal thickness ; Paraffin crystals ; Life and Medical Sciences ; Cell & Developmental Biology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Natural Sciences in General
    Notes: In the 3-dimensional (3-D) reconstruction of protein crystals with variable thicknesses the electron images and diffraction patterns can only be merged if the crystal thickness is known. Measurement of the thickness using the ratio of the number of inelastically scattered electrons to the number of electrons in the zero loss peak can be accomplished with parallel electron energy loss spectrometry (PEELS). A theoretical analysis of the accuracy of the technique on paraffin crystals of different thicknesses is presented. Our experimental studies with paraffin crystals show the feasibility of measuring a single layer of 47 Å with good accuracy under low dose and low temperature conditions. A simple experimental apparatus is proposed to obtain thicknesses from small regions of unstained protein crystals prior to collecting the 3-D data sets from the unexposed area of the same crystal.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    X-Ray Spectrometry 13 (1984), S. 55-59 
    ISSN: 0049-8246
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The total cross-sections for ionization of K, L and M shells in various atoms have been calculated using first-order perturbation theory and Hartree-Slater wave functions. For K shells, the hydrogenic wave functions have been used. The systematic changes across the Periodic Table are discussed and the results of a Bethe parametrization are also given.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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