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  • 1
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The high-brilliance, insertion-device-based photon beams of the next generation of synchrotron sources (Argonne's APS and Grenoble's ESRF) will deliver large thermal loads (1–10 kW) to the first optical elements. Considering the problems that present synchrotron users are experiencing with beams from recently installed insertion devices, new and improved methods of cooling these first optical elements, particularly when they are diffraction crystals, are clearly needed. A series of finite element calculations were performed to test the efficiency of new cooling geometries and various cooling fluids. The best results were obtained with liquid Ga metal flowing in channels just below the surface of the crystal. Ga was selected because of its good thermal conductivity and thermal capacity, low melting point, high boiling point, low kinetic viscosity, and very low vapor pressure. Its very low vapor pressure, even at elevated temperatures, makes it especially attractive in UHV conditions. A series of experiments were conducted at CHESS in February of 1988 that compared liquid gallium-cooled silicon diffraction crystals with water-cooled crystals. A six-pole wiggler beam was used to perform these tests on three different Si crystals, two with new cooling geometries and the one presently in use. A special high-pressure electromagnetic induction pump, recently developed at Argonne, was used to circulate the liquid gallium through the silicon crystals. In all experiments, the specially cooled crystal was used as the first crystal in a two crystal monochromator. An infrared camera was used to monitor the thermal profiles and correlated them with rocking curve measurements. A second set of cooling experiments were conducted in June of 1988 that used the intense, highly collimated beam from the newly installed ANL/CHESS undulator. Tests were performed on two new Ga-cooled Si crystals and compared with the standard water-cooled Si crystal. One of the crystals had cooling channels at two levels in the crystal that allowed one to actively control the shape of the crystal surface. The second one had rectangular cooling channels located just beneath the diffraction surface. Both crystals showed major improvements over the water-cooled crystal.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 63 (1992), S. 1746-1754 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The x-ray beams for the next generation of synchrotrons will contain much more power (1–10 kW) than is available at present day facilities. Cooling the first optical components in these beam lines will require the best cooling technology that one can bring to bear. Argonne continues to pioneer the use of liquid metals as the cooling fluid and has adopted liquid gallium as the liquid metal of choice. Its low melting point, 29.7 °C and its very low vapor pressure make it an easy fluid to handle and its high thermal conductivity and heat capacity make it an excellent cooling fluid. A series of experiments were performed during April 1991 with the wiggler beam at the F2 station of the CHESS facility at Cornell to investigate the cooling of large areas of high power. Two types of cooling crystal geometries were tested. One where the cooling channels were core drilled just below the surface of the crystal and a second where slots were cut into the crystal just below the surface with a diamond saw. Both crystals performed well with photon beam powers up to 1050 W and power densities of up to 14.5 W/mm2 at normal incidence. An infrared camera was used to measure the variation in the temperature of the top layer of the silicon crystals. For the core-drilled crystal the peak temperature measured at the center of the beam at a power density of 12.3 W/mm2 was 15 °C hotter than the crystal surface outside of the beam with a flow of liquid gallium of 2 gpm (gallons per minute) and was 10 °C with a flow of 4 gpm. The maximum distortion of the crystal surface distortion of the core-drilled crystal was about ±2.0 arcsec for the 2 gpm case with a maximum power density of 10.9 W/mm2 and about 5% of the expected beam intensity was lost at peak power of 14.5 W/mm2. For the slotted crystal the peak temperature difference for a peak power of 10.9 W/mm2 was 3.5 °C and 2.0 °C for liquid gallium flows of 1 gpm and 2 gpm, respectively. No intensity loss was measured for the maximum power density of 14.5 W/mm2. The fact that the peak temperature difference on the surface of both crystals was decreasing with increased flow of liquid gallium suggests that even higher power densities can be accommodated with higher flows of liquid gallium.
    Type of Medium: Electronic Resource
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  • 3
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: The x-ray beams for the next generation of synchrotrons will contain much more power (1–10 kW) than is available at present day facilities. Cooling the first optical components in these beam lines will require the best cooling technology that one can bring to bear. Argonne continues to pioneer the use of liquid metals as the cooling fluid and has adopted liquid gallium as the liquid metal of choice. Its low melting point, 29.7 °C and its very low vapor pressure make it an easy fluid to handle and its high thermal conductivity and heat capacity make it an excellent cooling fluid. A series of experiments were performed during April 1991 with the wiggler beam at the F2 station of the CHESS facility at Cornell to investigate the cooling of large areas of high power. Two types of cooling crystal geometries were tested, one where the cooling channels were core-drilled just below the surface of the crystal and a second where slots were cut into the crystal just below the surface with a diamond saw. Both crystals performed well with beam powers up to 1050 W and power densities of up to 14.5 W/mm2 at normal incidence.An infrared camera was used to measure the variation in the temperature of the top layer of the silicon crystals. For the core-drilled crystal the peak temperature measured at the center of the beam at a power density of 12.3 W/mm2 was 15 °C hotter than the crystal surface outside of the beam with a flow of liquid gallium of 2 gpm (gallons per minute) and was 10 °C with a flow of 4 gpm. The maximum distortion of the crystal surface distortion of the core drilled crystal was about ±2.0 arcsec for the 2 gpm case with a maximum power density of 10.9 W/mm2 and about 5% of the expected beam intensity was lost at peak power of 14.5 W/mm2. For the slotted crystal the peak temperature difference for a peak power of 10.9 W/mm2 was 3.5 and 2.0 °C for liquid gallium flows of 1 and 2 gpm, respectively. No intensity loss was measured for the maximum power density of 14.5 W/mm2. The fact that the peak temperature differences on the surface of both crystals was decreasing with increased flow of liquid gallium suggests that even higher power densities can be accommodated with higher flows of liquid gallium. This work is supported by the Department of Energy, BES-Materials Sciences, under Contract W-31-109-Eng-38.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 60 (1989), S. 2044-2047 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A new method has been developed to control the shape of the surface of a diffracting crystal that will allow it to function as a variable focus crystal diffraction lens for focusing photon beams from a synchrotron source. The new method uses thermal gradients in the crystal to control the shape of the surface of the crystal in two dimensions and allows one to generate both spherical and ellipsoidal surface shapes. In this work the thermal gradient was generated by core drilling two sets of cooling channels in a silicon crystal so that cooling or heating fluids could be circulated through the crystal at two different levels. The first set of channels is close to the surface of the crystal where the photon beam strikes it. The second set of channels is equidistant from the back surface. If a concave surface is desired, the fluid in the channels just below the surface exposed to the beam is cooler than the fluid circulating through the channels near the back surface. If a convex surface is desired, then the cooling fluid in the upper channels near the surface exposed to the incident photon beam is warmer than the fluid in the lower channels. The focal length of the crystal lens is varied by varying the thermal gradient in the crystal. This approach can also be applied to the first crystal in a high power synchrotron beamline to eliminate the bowing and other thermal distortions of the crystal caused by the high heat load.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    [s.l.] : Nature Publishing Group
    Nature 306 (1983), S. 94-95 
    ISSN: 1476-4687
    Source: Nature Archives 1869 - 2009
    Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics
    Notes: [Auszug] IT MIGHT seem odd that one of the first two books in this promising series on various aspects of biotechnology should deal with patent aspects, but one of the most important driving forces for research in this area is the possibility of commercial exploitation. The second book, more in line with ...
    Type of Medium: Electronic Resource
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  • 6
    ISSN: 1434-601X
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract A πh 11 2/3 level spectrum and other lowlying yrast states in149Ho have been identified in reactions of 155–180 MeV32S with121Sb and122Te targets. The results agree well with shell model predictions.
    Type of Medium: Electronic Resource
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  • 7
    ISSN: 0884-3996
    Keywords: Luminometer ; evaluation ; rapid microbiology ; ATP assay ; firefly luciferase ; photometer ; radiometer ; comparison ; Chemistry ; Biochemistry and Biotechnology
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Biology , Chemistry and Pharmacology
    Notes: An assessment has been carried out of the relative performance of ten instruments for quantification of adenosine triphosphate (ATP) by the firefly luciferase assay. The instruments evaluated were Amersham Amerlite Analyser, Dynatech Tube Luminometer, Dynatech Multiplate Luminometer, Dynatech Camera Luminometer, Hamilton Lumicon, LKB 1250 Luminometer, LKB 1251 Luminometer, Lumac Biocounter M2010A, Turner 20 TD Luminometer and a prototype version of the CLEAR Speed Tech 2000. An 800-fold difference in sensitivity was found between the most sensitive (Lumac, Turner) and the least sensitive (Dynatech Tube) of the conventional instruments. The Dynatech Camera Luminometer which worked on a completely different principle to the other instruments was about 5000 times less sensitive than the best of the photomultiplier tube instruments. The relative sensitivity of the instruments was maintained regardless of whether solutions of ATP in water or trichloroacetic acid extracts of bacteria were analysed. An analysis of 960 ATP bioluminescence assays showed that data obtained from such measurements are normally distributed.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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