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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : International Union of Crystallography (IUCr)
    Acta crystallographica 43 (1987), S. 131-133 
    ISSN: 1600-5724
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Notes: Part of the diffraction pattern of a single biological cell (diatom) has been observed using 32 Å synchrotron X-rays.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 60 (1989), S. 214-218 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Recently, several x-ray techniques have been demonstrated to have unique capabilities of making microscopic measurement on a monolayer supported on a liquid subphase. Substantial information about the phase transitions and chemical reactions of the monolayer system previously unavailable has been obtained. In this paper a Langmuir trough designed to perform these x-ray experiments is described. Design considerations specific for the x-ray applications are discussed, and the hardware implementation is described. The trough has been used successfully in our monolayer study using surface extended x-ray absorption fine structure (SEXAFS) and near total external fluorescence (NTEF) techniques.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 68 (1990), S. 1421-1428 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The synchrotron x-ray near total external fluorescence technique is used to measure the concentration profiles of elements near a sample surface along its surface normal. This novel nondestructive technique is capable of providing information about the concentration profiles on a length scale of tens to hundreds of angstroms from the sample surface. It does not require vacuum and can be applied at ambient pressures. Concentration profiles of virtually all the elements in the periodic table can be investigated using this technique. The lower limit of detection is approximately equivalent to (1)/(10) of a monolayer coverage. The technique is particularly useful in applications where the fluorescence signal originating from a thin surface layer can be normalized against that originating from the same element in the bulk of the sample. The experimental procedure and the data analysis are demonstrated using experimental results of metal-ion segregation from a liquid solution to a liquid/air interface.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 71 (1992), S. 5709-5711 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We present a novel application of the Fresnel zone plate geometry in which the Mössbauer effect is used to focus nuclear-resonant x-ray photons and thereby to monochromatize synchrotron radiation. The calculated efficiency and energy bandpass of the Mössbauer–Fresnel zone plate monochromator compare well with those of other Mössbauer-effect monochromators currently in use. The unique capability of focusing Mössbauer radiation into a small (few μm) spot may have applications in spatially resolved and high-pressure Mössbauer-effect studies.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 64 (1993), S. 858-863 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A tapered undulator, in which the entrance and exit magnetic gaps are different, will show an increase in the energy width of the harmonics compared to the nontapered case. This increase can occur without substantial broadening in the collimation of the undulator radiation. We present the spectral properties measured for a tapered 3.3-cm period prototype undulator of the Advanced Photon Source at the Cornell High Energy Synchrotron Source. The width of the on-axis first harmonic at 6.9 keV increased from 0.32 to 0.66 keV for a gap tapering of 12%. Minimal angular broadening in the first harmonic x rays was detected and measurements of off-axis radiation were also performed. The results are found to be in good agreement with model calculations.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 63 (1992), S. 582-585 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Coherent hard x-ray beams with a flux exceeding 109 photons/sec with a bandwidth of 0.1% will be provided by undulators at the third-generation synchrotron radiation sources such as APS, ESRF, and Spring-8. The availability of such high flux coherent x-ray beams offers excellent opportunities for extending the coherence-based techniques developed in the visible and soft x-ray part of the electromagnetic spectrum to the hard x-ray region. These x-ray techniques (e.g., diffraction-limited microfocusing, holography, interferometry, phase contrast imaging, and signal enhancement) may offer substantial advantages over noncoherence-based x-ray techniques currently used. For example, the signal-enhancement technique may be used to enhance an anomalous x-ray or magnetic x-ray scattering signal by several orders of magnitude. Coherent x rays can be focused to a very small (diffraction-limited) spot size, thus allowing construction of high spatial resolution microprobes. This paper will discuss the feasibility of extending some coherence-based techniques to the hard x-ray range and the significant progress that has been made in the development of diffraction-limited focusing optics. Specific experimental results for a transmission Fresnel phase zone plate that can focus 8.2 keV x rays to a spot size of about 2 microns will be briefly discussed. The comparison of measured focusing efficiency of the zone plate with that calculated will be made. Some specific applications of zone plates as coherent x-ray optics will be discussed.
    Type of Medium: Electronic Resource
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  • 7
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A Fresnel phase zone plate with an unprecedented focusing efficiency of 33% was fabricated using an x-ray lithographic technique and was tested using synchrotron x rays. Contributions by the zeroth-order x ray to the focus were minimal. Spatial resolution in the micrometer range was achieved. The measured spot size was dominated by geometric demagnification of the source. It should be possible to obtain submicrometer resolution by aperturing the source. Experimental results of focusing efficiency measurements, intensity distribution at the focal plane, and spatial resolution tests are reported.
    Type of Medium: Electronic Resource
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